About: Reaction of 9-acridinylisothiocyanate with methyl- and phenylhydrazine     Goto   Sponge   NotDistinct   Permalink

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  • The acridinyl thioureas (I) give S-methylated and S,N-dimethylated products, while the thioureas (II) provide only Smethylated derivative at the same conditions. The ab initio calculation was used to determine the moust favorable structural isomers, tautomeric structures and intramolecular interactions. The structural elucidation of synthetized derivatives was accomplished by 1H, 13C NMR spectroscopy (PDQF-COSY, selective INEPT, NOE). Among studied compounds (I-IV), acridinium salts of S(N)dimethylisothioureas (III) exhibited the highest intensity of fluorescence and biological activity against Mycobacterium tuberculosis.
  • The acridinyl thioureas (I) give S-methylated and S,N-dimethylated products, while the thioureas (II) provide only Smethylated derivative at the same conditions. The ab initio calculation was used to determine the moust favorable structural isomers, tautomeric structures and intramolecular interactions. The structural elucidation of synthetized derivatives was accomplished by 1H, 13C NMR spectroscopy (PDQF-COSY, selective INEPT, NOE). Among studied compounds (I-IV), acridinium salts of S(N)dimethylisothioureas (III) exhibited the highest intensity of fluorescence and biological activity against Mycobacterium tuberculosis. (en)
Title
  • Reaction of 9-acridinylisothiocyanate with methyl- and phenylhydrazine
  • Reaction of 9-acridinylisothiocyanate with methyl- and phenylhydrazine (en)
skos:prefLabel
  • Reaction of 9-acridinylisothiocyanate with methyl- and phenylhydrazine
  • Reaction of 9-acridinylisothiocyanate with methyl- and phenylhydrazine (en)
skos:notation
  • RIV/60461373:22310/03:00007874!RIV/2004/MSM/223104/N
http://linked.open.../vavai/riv/strany
  • 759
http://linked.open...avai/riv/aktivita
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  • Z(MSM 223100001)
http://linked.open...iv/cisloPeriodika
  • 8
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  • 624629
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  • RIV/60461373:22310/03:00007874
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  • acridinyl thioureas (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • CZ - Česká republika
http://linked.open...ontrolniKodProRIV
  • [5CD782D06890]
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  • Chemické listy
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http://linked.open...v/svazekPeriodika
  • 97
http://linked.open...iv/tvurceVysledku
  • Böhm, Stanislav
  • Balentová, E.
  • Bernát, J.
  • Baranová, J.
  • Bušová, T.
  • Danihel, I.
http://linked.open...n/vavai/riv/zamer
issn
  • 0009-2770
number of pages
http://localhost/t...ganizacniJednotka
  • 22310
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