About: Determination of Selected Beer Flavours: Comparison of a Stir Bar Sorptive Extraction and a Steam Distillation Procedure     Goto   Sponge   NotDistinct   Permalink

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  • The aim of this work was focused on the comparison of two sample preparation procedures – a stir bar sorptive extraction (SBSE) followed by solvent back extraction and a well-established distillation method followed by liquid/liquid extraction – for the simultaneous determination of some beer esters (isoamyl acetate, ethyl caproate, ethyl caprylate, ethyl caprate, phenylethyl acetate, ethyl laurate, ethyl myristate, ethyl palmitate) and free fatty acids (caproic, caprylic, pelargonic, capric). Subsequent gas chromatographic analyses with flame ionization detection were used for the determination of these compounds. Both procedures were characterized by good linearity (correlation coefficients were higher than 0.9987). The relative standard deviations were found to be 2.1–7.3% for SBSE and 10–14% for the distillation technique with recovery 81–107% and 70–89%, respectively. Results obtained by these two procedures were in good correlation.
  • The aim of this work was focused on the comparison of two sample preparation procedures – a stir bar sorptive extraction (SBSE) followed by solvent back extraction and a well-established distillation method followed by liquid/liquid extraction – for the simultaneous determination of some beer esters (isoamyl acetate, ethyl caproate, ethyl caprylate, ethyl caprate, phenylethyl acetate, ethyl laurate, ethyl myristate, ethyl palmitate) and free fatty acids (caproic, caprylic, pelargonic, capric). Subsequent gas chromatographic analyses with flame ionization detection were used for the determination of these compounds. Both procedures were characterized by good linearity (correlation coefficients were higher than 0.9987). The relative standard deviations were found to be 2.1–7.3% for SBSE and 10–14% for the distillation technique with recovery 81–107% and 70–89%, respectively. Results obtained by these two procedures were in good correlation. (en)
Title
  • Determination of Selected Beer Flavours: Comparison of a Stir Bar Sorptive Extraction and a Steam Distillation Procedure
  • Determination of Selected Beer Flavours: Comparison of a Stir Bar Sorptive Extraction and a Steam Distillation Procedure (en)
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  • Determination of Selected Beer Flavours: Comparison of a Stir Bar Sorptive Extraction and a Steam Distillation Procedure
  • Determination of Selected Beer Flavours: Comparison of a Stir Bar Sorptive Extraction and a Steam Distillation Procedure (en)
skos:notation
  • RIV/60193697:_____/11:#0000638!RIV12-MSM-60193697
http://linked.open...avai/riv/aktivita
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  • I, Z(MSM6019369701)
http://linked.open...iv/cisloPeriodika
  • 4
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http://linked.open...aciTvurceVysledku
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  • 193882
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  • RIV/60193697:_____/11:#0000638
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  • beer; beer flavours; gas chromatography; stir bar (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV
  • [B44F26D1B038]
http://linked.open...i/riv/nazevZdroje
  • Journal of The Institute of Brewing
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http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 117
http://linked.open...iv/tvurceVysledku
  • Dvořák, Josef
  • Horák, Tomáš
  • Kellner, Vladimír
  • Čejka, Pavel
  • Hašková, Danuša
  • Jurková, Marie
  • Čulík, Jiří
http://linked.open...n/vavai/riv/zamer
issn
  • 0046-9750
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