About: Development of solid-phase extraction and HPLC-MS methods for deoxinivalenol determination in barley and malt

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About: Development of solid-phase extraction and HPLC-MS methods for deoxinivalenol determination in barley and malt Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Method for the determination of deoxinivalenol (DON) in cereals has been developed and applied. Solid phase extraction with Envicarb cleans up columns and subsequent separation by HPLC-MS and C-18 Luna (Phenomenex, USA) column. DON was detected by MS in positive mode. The developed method is relatively cheap and fast with high sensitivity. The method was used for determination of DON in barley and malt. The detection limit for barley was 25 µg/kg and for malt it was 30 µg/kg. A variation in quantity of DON in samples after a malting process was found. Method for the determination of deoxinivalenol (DON) in cereals has been developed and applied. Solid phase extraction with Envicarb cleans up columns and subsequent separation by HPLC-MS and C-18 Luna (Phenomenex, USA) column. DON was detected by MS in positive mode. The developed method is relatively cheap and fast with high sensitivity. The method was used for determination of DON in barley and malt. The detection limit for barley was 25 µg/kg and for malt it was 30 µg/kg. A variation in quantity of DON in samples after a malting process was found. (en)
Title	Development of solid-phase extraction and HPLC-MS methods for deoxinivalenol determination in barley and malt Development of solid-phase extraction and HPLC-MS methods for deoxinivalenol determination in barley and malt (en)
skos:prefLabel	Development of solid-phase extraction and HPLC-MS methods for deoxinivalenol determination in barley and malt Development of solid-phase extraction and HPLC-MS methods for deoxinivalenol determination in barley and malt (en)
skos:notation	RIV/60162694:G44__/09:00002129!RIV10-MO0-G44_____
http://linked.open...avai/riv/aktivita	P S Z
http://linked.open...avai/riv/aktivity	P(OPUOFVZ200604), S, Z(MSM2532885901)
http://linked.open...iv/cisloPeriodika	8
http://linked.open...vai/riv/dodaniDat	2010
http://linked.open...aciTvurceVysledku	Žďárová Karasová, Jana
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Ministerstvo obrany / Univerzita obrany - Fakulta vojenského zdravotnictví Hradec Králové
http://linked.open...dnocenehoVysledku	351163
http://linked.open...ai/riv/idVysledku	RIV/60162694:G44__/09:00002129
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	deoxinivalenol; mycotoxin; HPLC-MS; barley; malt (en)
http://linked.open.../riv/klicoveSlovo	HPLC-MS barley malt mycotoxin deoxinivalenol
http://linked.open...odStatuVydavatele	CZ - Česká republika
http://linked.open...ontrolniKodProRIV	[BFBCD35BC277]
http://linked.open...i/riv/nazevZdroje	Chemické listy
http://linked.open...in/vavai/riv/obor	FP
http://linked.open...ichTvurcuVysledku	1 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...vavai/riv/projekt	Biological indicators of ionizing radiation
http://linked.open...UplatneniVysledku	2009
http://linked.open...v/svazekPeriodika	103
http://linked.open...iv/tvurceVysledku	Dohnal, Vlastimil Polišenská, Ivana Žďárová Karasová, Jana Ježková, Alena
http://linked.open...ain/vavai/riv/wos	000269243500009
http://linked.open...n/vavai/riv/zamer	Optimisation of sustainability factors of crop production based on the development of genetic and breeding, diagnostic and decision-making methods
issn	0009-2770
number of pages	5 (xsd:int)
http://localhost/t...ganizacniJednotka	G44

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