About: Heterogeneous phase formation in diluted magnetic semiconducting Zn1-x-yCoxAlyO (CAZO) nanoparticles     Goto   Sponge   NotDistinct   Permalink

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  • This article reports a systematic investigation of the synthesis and structural characterization of a composite CAZO [(Zn1?x?yCoxAlyO; x=0.04, 0.03, 0.02; y=0.01, 0.02, 0.03)] nanoparticles from combustion. The crystalline phase, morphology, size, and structure were characterized using X-ray diffraction (XRD), small and wide angle X-ray scattering (SAXS/WAXS), scanning electron microscopy (SEM) and high resolution transmission electron microscopy (HR-TEM). The XRD and SAXS/WAXS analyses confirm the formation of Co and Al co-doped ZnO hexagonal wurtzite structure with additional metal oxides phase. The particle size and micro-strain were calculated by means of an integral breadth of X-ray diffraction lines. The selected area electron diffraction (SAED) patterns from TEM were correlated with the XRD patterns. The energy dispersive X-ray spectra (EDX) from SEM/TEM were recorded in order to analyze the composition of elements in the composite. The vibrational modes of the functional groups presented in the materials were assigned from FTIR and Raman spectra. The magnetic hysteresis measurement confirmed the room temperature ferromagnetism.
  • This article reports a systematic investigation of the synthesis and structural characterization of a composite CAZO [(Zn1?x?yCoxAlyO; x=0.04, 0.03, 0.02; y=0.01, 0.02, 0.03)] nanoparticles from combustion. The crystalline phase, morphology, size, and structure were characterized using X-ray diffraction (XRD), small and wide angle X-ray scattering (SAXS/WAXS), scanning electron microscopy (SEM) and high resolution transmission electron microscopy (HR-TEM). The XRD and SAXS/WAXS analyses confirm the formation of Co and Al co-doped ZnO hexagonal wurtzite structure with additional metal oxides phase. The particle size and micro-strain were calculated by means of an integral breadth of X-ray diffraction lines. The selected area electron diffraction (SAED) patterns from TEM were correlated with the XRD patterns. The energy dispersive X-ray spectra (EDX) from SEM/TEM were recorded in order to analyze the composition of elements in the composite. The vibrational modes of the functional groups presented in the materials were assigned from FTIR and Raman spectra. The magnetic hysteresis measurement confirmed the room temperature ferromagnetism. (en)
Title
  • Heterogeneous phase formation in diluted magnetic semiconducting Zn1-x-yCoxAlyO (CAZO) nanoparticles
  • Heterogeneous phase formation in diluted magnetic semiconducting Zn1-x-yCoxAlyO (CAZO) nanoparticles (en)
skos:prefLabel
  • Heterogeneous phase formation in diluted magnetic semiconducting Zn1-x-yCoxAlyO (CAZO) nanoparticles
  • Heterogeneous phase formation in diluted magnetic semiconducting Zn1-x-yCoxAlyO (CAZO) nanoparticles (en)
skos:notation
  • RIV/49777513:23640/14:43922261!RIV15-MSM-23640___
http://linked.open...avai/riv/aktivita
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  • I, P(ED2.1.00/03.0088)
http://linked.open...iv/cisloPeriodika
  • 45
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  • 18997
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  • RIV/49777513:23640/14:43922261
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  • Magnetic properties.; Raman spectroscopy; HR-TEM; microstructure; SAXS/WAXS; CAZO nanoparticles (en)
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  • GB - Spojené království Velké Británie a Severního Irska
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  • [404F0EEC0B20]
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  • 4
http://linked.open...iv/tvurceVysledku
  • David, Bohumil
  • Očenášek, Jan
  • Šutta, Pavol
  • Medlín, Rostislav
  • Bělský, Petr
  • Vavruňková, Veronika
  • Rajendran, Siddheswaran
issn
  • 2046-2069
number of pages
http://bibframe.org/vocab/doi
  • 10.1039/C4RA02973A
http://localhost/t...ganizacniJednotka
  • 23640
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