About: Isolation of Biogenic Amines Using Paramagnetic Microparticles Off-Line Coupled with Ion Exchange Liquid Chromatography     Goto   Sponge   NotDistinct   Permalink

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  • This study aims at the possibility of single structured paramagnetic microparticles (PMPs), composed of maghemite (y-Fe2O3) core modified with chitosan called MAN8, or tetraethyl orthosilicate covered with Dowex called MAN35, to be helpful for isolation of biogenic amines prior to their further analysis. Primarily, we synthesized and characterized PMPs. To obtain the information about bead morphology, scanning electron microscopy was employed. Furthermore, X-ray fluorescence was employed to carry out the elemental composition analyses. To obtain further insight into interaction between PMP surface and biogenic amines, scanning electron microscope was employed. It was shown that binding of biogenic amines causes increase of relative current response of deprotonated microparticles. We tested the specificity of PMPs to bind biogenic amines on histamine, tyramine, spermine, spermidine, putrescine, and cadaverine. We found that two types of our PMPs were able to selectively bind spermidine, cadaverine, and
  • This study aims at the possibility of single structured paramagnetic microparticles (PMPs), composed of maghemite (y-Fe2O3) core modified with chitosan called MAN8, or tetraethyl orthosilicate covered with Dowex called MAN35, to be helpful for isolation of biogenic amines prior to their further analysis. Primarily, we synthesized and characterized PMPs. To obtain the information about bead morphology, scanning electron microscopy was employed. Furthermore, X-ray fluorescence was employed to carry out the elemental composition analyses. To obtain further insight into interaction between PMP surface and biogenic amines, scanning electron microscope was employed. It was shown that binding of biogenic amines causes increase of relative current response of deprotonated microparticles. We tested the specificity of PMPs to bind biogenic amines on histamine, tyramine, spermine, spermidine, putrescine, and cadaverine. We found that two types of our PMPs were able to selectively bind spermidine, cadaverine, and (en)
Title
  • Isolation of Biogenic Amines Using Paramagnetic Microparticles Off-Line Coupled with Ion Exchange Liquid Chromatography
  • Isolation of Biogenic Amines Using Paramagnetic Microparticles Off-Line Coupled with Ion Exchange Liquid Chromatography (en)
skos:prefLabel
  • Isolation of Biogenic Amines Using Paramagnetic Microparticles Off-Line Coupled with Ion Exchange Liquid Chromatography
  • Isolation of Biogenic Amines Using Paramagnetic Microparticles Off-Line Coupled with Ion Exchange Liquid Chromatography (en)
skos:notation
  • RIV/00216305:26620/14:PU112639!RIV15-MSM-26620___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • I, S
http://linked.open...iv/cisloPeriodika
  • 21-22
http://linked.open...vai/riv/dodaniDat
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  • 22957
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  • RIV/00216305:26620/14:PU112639
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  • Biogenic amines, Biosensor, Ion-exchange liquid chromatography, Magnetic-particles-based separation (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [05F61C07ADA4]
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  • CHROMATOGRAPHIA
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  • 77
http://linked.open...iv/tvurceVysledku
  • Adam, Vojtěch
  • Cernei, Natalia Vladimirovna
  • Kizek, René
  • Skládanka, Jiří
  • Zítka, Ondřej
  • Kopel, Pavel
  • Heger, Zbyněk
issn
  • 0009-5893
number of pages
http://bibframe.org/vocab/doi
  • 10.1007/s10337-014-2731-8
http://localhost/t...ganizacniJednotka
  • 26620
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