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  • The aim of the work was to develop and validate a new simplified procedure for isolation of benzo[a]pyrene (BaP) from smoked sausages. The procedure was elaborated application extraction and clean-up operation in just one-step, thus avoiding losses of analyte and saving time. To eliminate post-extraction clean-up step, silica gel as sorbent was applied directly to the ASE extraction cell to prevent the extraction of interfering compounds into BaP fraction. The procedure was studied at three concentration levels – 0.4, 5, and 10 mikrog.kg-1 when the sample was spiked with BaP, placed into extraction cell on sorbent layer and extracted with n-hexane at 100 centigrades and 10 for 10 min. The flush volume was 60% and the purge time 120 s. One static cycle was accomplished three times. The solvent of the extract was evaporated in a water bath using a nitrogen stream. Then residuum was dissolved in methanol and analysed by HPLC with FLD. On the base of measured data, parameters of the method are as follo
  • The aim of the work was to develop and validate a new simplified procedure for isolation of benzo[a]pyrene (BaP) from smoked sausages. The procedure was elaborated application extraction and clean-up operation in just one-step, thus avoiding losses of analyte and saving time. To eliminate post-extraction clean-up step, silica gel as sorbent was applied directly to the ASE extraction cell to prevent the extraction of interfering compounds into BaP fraction. The procedure was studied at three concentration levels – 0.4, 5, and 10 mikrog.kg-1 when the sample was spiked with BaP, placed into extraction cell on sorbent layer and extracted with n-hexane at 100 centigrades and 10 for 10 min. The flush volume was 60% and the purge time 120 s. One static cycle was accomplished three times. The solvent of the extract was evaporated in a water bath using a nitrogen stream. Then residuum was dissolved in methanol and analysed by HPLC with FLD. On the base of measured data, parameters of the method are as follo (en)
Title
  • New simplified procedure for isolation of benzo[a]pyrene from smoked sausages.
  • New simplified procedure for isolation of benzo[a]pyrene from smoked sausages. (en)
skos:prefLabel
  • New simplified procedure for isolation of benzo[a]pyrene from smoked sausages.
  • New simplified procedure for isolation of benzo[a]pyrene from smoked sausages. (en)
skos:notation
  • RIV/00216305:26310/13:PU104471!RIV14-MSM-26310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • S
http://linked.open...iv/cisloPeriodika
  • 2
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
  • Šimko, Peter
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 91685
http://linked.open...ai/riv/idVysledku
  • RIV/00216305:26310/13:PU104471
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Accelerated solvent extraction, polycyclic aromatic hydrocarbons, benzo[a]pyrene, smoked sausages, HPLC (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • SK - Slovenská republika
http://linked.open...ontrolniKodProRIV
  • [7389ADB7E451]
http://linked.open...i/riv/nazevZdroje
  • Journal of Food and Nutrition Research
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 52
http://linked.open...iv/tvurceVysledku
  • Šimko, Peter
issn
  • 1336-8672
number of pages
http://localhost/t...ganizacniJednotka
  • 26310
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