About: Simultaneous Determination of Inorganic Arsenic, Antimony, Selenium and Tellurium by ICP-MS in Environmental Waters Using SPE Preconcentration on Modified Silica.

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About: Simultaneous Determination of Inorganic Arsenic, Antimony, Selenium and Tellurium by ICP-MS in Environmental Waters Using SPE Preconcentration on Modified Silica. Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	This paper deals with a simplified multielement profiling of inorganic arsenic, antimony, selenium and tellurium in the form of 75As, 82Se, 121Sb and 125Te by ICP-MS for amounts less than 10 ug/L. Internal standards such as 72Ge and 209Bi were successfully used for the suppression of both influence of macro elements Na+, K+, Ca2+, Mg2+ or Al3+, and interference of limited concentrations of heavy metal ions. Modified silica sorbents Separon SGX C18, C8, CN, NH2, RPS and Phenyl were tested for the preconcentration of As, Sb, Se and Te (0.25-5 ug/L) in the form of ion associates with cationic surfactants from 50-250 mL sample volume. 1-etoxycarbonyl-pentadecyltrimethylammonium bromide (Septonex 0.005 mol/L) was suitable for this purpose in the presence of 4-(2-pyridylazo) resorcinol, 2-pyrrolidinecarbodithioate and 8-hydroxyquinoline-5-sulphonic acid. The quantitative retention occurred at pH 7 and the mixture of acetone with ethanol in ratio 1:1 in the presence of 0,1 mol/L HCl was used for the quantit This paper deals with a simplified multielement profiling of inorganic arsenic, antimony, selenium and tellurium in the form of 75As, 82Se, 121Sb and 125Te by ICP-MS for amounts less than 10 ug/L. Internal standards such as 72Ge and 209Bi were successfully used for the suppression of both influence of macro elements Na+, K+, Ca2+, Mg2+ or Al3+, and interference of limited concentrations of heavy metal ions. Modified silica sorbents Separon SGX C18, C8, CN, NH2, RPS and Phenyl were tested for the preconcentration of As, Sb, Se and Te (0.25-5 ug/L) in the form of ion associates with cationic surfactants from 50-250 mL sample volume. 1-etoxycarbonyl-pentadecyltrimethylammonium bromide (Septonex 0.005 mol/L) was suitable for this purpose in the presence of 4-(2-pyridylazo) resorcinol, 2-pyrrolidinecarbodithioate and 8-hydroxyquinoline-5-sulphonic acid. The quantitative retention occurred at pH 7 and the mixture of acetone with ethanol in ratio 1:1 in the presence of 0,1 mol/L HCl was used for the quantit (en)
Title	Simultaneous Determination of Inorganic Arsenic, Antimony, Selenium and Tellurium by ICP-MS in Environmental Waters Using SPE Preconcentration on Modified Silica. Simultaneous Determination of Inorganic Arsenic, Antimony, Selenium and Tellurium by ICP-MS in Environmental Waters Using SPE Preconcentration on Modified Silica. (en)
skos:prefLabel	Simultaneous Determination of Inorganic Arsenic, Antimony, Selenium and Tellurium by ICP-MS in Environmental Waters Using SPE Preconcentration on Modified Silica. Simultaneous Determination of Inorganic Arsenic, Antimony, Selenium and Tellurium by ICP-MS in Environmental Waters Using SPE Preconcentration on Modified Silica. (en)
skos:notation	RIV/00216305:26310/11:PU92210!RIV12-MSM-26310___
http://linked.open...avai/riv/aktivita	S
http://linked.open...avai/riv/aktivity	S
http://linked.open...iv/cisloPeriodika	11
http://linked.open...vai/riv/dodaniDat	2012
http://linked.open...aciTvurceVysledku	Moos, Martin Sommer, Lumír
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Vysoké učení technické v Brně / Fakulta chemická
http://linked.open...dnocenehoVysledku	229519
http://linked.open...ai/riv/idVysledku	RIV/00216305:26310/11:PU92210
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	arsenic, antimony, selenium, tellurium, solid-phase extraction (SPE), ICP-MS, waters (en)
http://linked.open.../riv/klicoveSlovo	arsenic ICP-MS solid-phase extraction (SPE) tellurium waters selenium antimony
http://linked.open...odStatuVydavatele	GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV	[34C7E45E7FC5]
http://linked.open...i/riv/nazevZdroje	International Journal of Environmental Analytical Chemistry
http://linked.open...in/vavai/riv/obor	CB
http://linked.open...ichTvurcuVysledku	2 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...UplatneniVysledku	2011
http://linked.open...v/svazekPeriodika	91
http://linked.open...iv/tvurceVysledku	Machát, Jiří Moos, Martin Sommer, Lumír Urbánková, Kristýna
issn	1029-0397
number of pages	10 (xsd:int)
http://localhost/t...ganizacniJednotka	26310

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