About: Lead Film Electrode Prepared with the Use of a Reversibly Deposited Mediator Metal in Adsorptive Stripping Voltammetry of Nickel     Goto   Sponge   NotDistinct   Permalink

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  • The paper presents the first report on application of a %22hybrid%22 lead film electrode for the adsorptive stripping voltammetric determination of Ni(II) in the presence of nioxime as a complexing agent. The strategy to create a %22hybrid%22 electrode is based on the combination of ex situ and in situ plating methods and the use of a reversibly deposited mediator metal (Zn) for the lead film formation. The surface morphology of a new sensor was characterized by atomic force microscopy. The detection limit for Ni(II) obtained at 120 s of accumulation time was 3.9 x 10(-11) mol L(-1). The proposed method was validated for the determination of nickel in water certified reference materials with good results.
  • The paper presents the first report on application of a %22hybrid%22 lead film electrode for the adsorptive stripping voltammetric determination of Ni(II) in the presence of nioxime as a complexing agent. The strategy to create a %22hybrid%22 electrode is based on the combination of ex situ and in situ plating methods and the use of a reversibly deposited mediator metal (Zn) for the lead film formation. The surface morphology of a new sensor was characterized by atomic force microscopy. The detection limit for Ni(II) obtained at 120 s of accumulation time was 3.9 x 10(-11) mol L(-1). The proposed method was validated for the determination of nickel in water certified reference materials with good results. (en)
Title
  • Lead Film Electrode Prepared with the Use of a Reversibly Deposited Mediator Metal in Adsorptive Stripping Voltammetry of Nickel
  • Lead Film Electrode Prepared with the Use of a Reversibly Deposited Mediator Metal in Adsorptive Stripping Voltammetry of Nickel (en)
skos:prefLabel
  • Lead Film Electrode Prepared with the Use of a Reversibly Deposited Mediator Metal in Adsorptive Stripping Voltammetry of Nickel
  • Lead Film Electrode Prepared with the Use of a Reversibly Deposited Mediator Metal in Adsorptive Stripping Voltammetry of Nickel (en)
skos:notation
  • RIV/00216275:25310/14:39898304!RIV15-MSM-25310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • I
http://linked.open...iv/cisloPeriodika
  • 9
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  • 25813
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  • RIV/00216275:25310/14:39898304
http://linked.open...riv/jazykVysledku
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  • adsorptive stripping voltammetry; Ni(II) determination; mediator metal; hybrid lead film electrode (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [95EE84D99F1A]
http://linked.open...i/riv/nazevZdroje
  • Electroanalysis
http://linked.open...in/vavai/riv/obor
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  • 26
http://linked.open...iv/tvurceVysledku
  • Metelka, Radovan
  • Vytřas, Karel
  • Tyszczuk-Rotko, Katarzyna
  • Barczak, Mariusz
http://linked.open...ain/vavai/riv/wos
  • 000343926700024
issn
  • 1040-0397
number of pages
http://bibframe.org/vocab/doi
  • 10.1002/elan.201400263
http://localhost/t...ganizacniJednotka
  • 25310
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