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Description
| - An analysis of the effects of dopants concentration and different starting titanium compounds on the anatase to rutile phase transformation at the synthesis of rutile pigments Ti1-3xCrxNb2xO2 +/-delta is presented in this study. The main goal was to analyze reaction mixtures for x = 0.05 (previous study) and 0.30 by simultaneous TG-DTA analysis and to determine the temperature of anatase-rutile transition. For x = 0.05, initial temperatures 760-830 A degrees C are needful for a formation of rutile structure. The temperature is the lowest for the hydrated Na2Ti4O9 paste (760 A degrees C) and similar for other starting compounds of titanium. But for x = 0.30, the anatase-rutile transition begins at higher temperatures 910-1,030 A degrees C because of high-Nb content, which is the inhibitor of this modification change. In addition, we found the influence of calcination temperatures (850, 900, 950, 1000, 1050, 1100, and 1150 A degrees C) on color properties and particle size distribution of these materials prepared from anatase TiO2 and with x = 0.30. Selected pigments were also analyzed by X-ray powder diffraction.
- An analysis of the effects of dopants concentration and different starting titanium compounds on the anatase to rutile phase transformation at the synthesis of rutile pigments Ti1-3xCrxNb2xO2 +/-delta is presented in this study. The main goal was to analyze reaction mixtures for x = 0.05 (previous study) and 0.30 by simultaneous TG-DTA analysis and to determine the temperature of anatase-rutile transition. For x = 0.05, initial temperatures 760-830 A degrees C are needful for a formation of rutile structure. The temperature is the lowest for the hydrated Na2Ti4O9 paste (760 A degrees C) and similar for other starting compounds of titanium. But for x = 0.30, the anatase-rutile transition begins at higher temperatures 910-1,030 A degrees C because of high-Nb content, which is the inhibitor of this modification change. In addition, we found the influence of calcination temperatures (850, 900, 950, 1000, 1050, 1100, and 1150 A degrees C) on color properties and particle size distribution of these materials prepared from anatase TiO2 and with x = 0.30. Selected pigments were also analyzed by X-ray powder diffraction. (en)
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Title
| - The Influence of Concentration of Doping Elements on Anatase-Rutile Transformation at the Synthesis of Rutile Pigments (Ti,Cr,Nb)O2 and their Pigmentary Properties
- The Influence of Concentration of Doping Elements on Anatase-Rutile Transformation at the Synthesis of Rutile Pigments (Ti,Cr,Nb)O2 and their Pigmentary Properties (en)
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skos:prefLabel
| - The Influence of Concentration of Doping Elements on Anatase-Rutile Transformation at the Synthesis of Rutile Pigments (Ti,Cr,Nb)O2 and their Pigmentary Properties
- The Influence of Concentration of Doping Elements on Anatase-Rutile Transformation at the Synthesis of Rutile Pigments (Ti,Cr,Nb)O2 and their Pigmentary Properties (en)
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skos:notation
| - RIV/00216275:25310/14:39897851!RIV15-MSM-25310___
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http://linked.open...avai/riv/aktivita
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http://linked.open...avai/riv/aktivity
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http://linked.open...iv/cisloPeriodika
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http://linked.open...vai/riv/dodaniDat
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http://linked.open...aciTvurceVysledku
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http://linked.open.../riv/druhVysledku
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http://linked.open...iv/duvernostUdaju
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http://linked.open...titaPredkladatele
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http://linked.open...dnocenehoVysledku
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http://linked.open...ai/riv/idVysledku
| - RIV/00216275:25310/14:39897851
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http://linked.open...riv/jazykVysledku
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http://linked.open.../riv/klicovaSlova
| - Particle Size Distribution; Color Properties; X-ray Powder Diffraction; Simultaneous TG-DTA Analysis; Anatase-Rutile Transformation; Rutile Pigments (en)
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http://linked.open.../riv/klicoveSlovo
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http://linked.open...odStatuVydavatele
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http://linked.open...ontrolniKodProRIV
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http://linked.open...i/riv/nazevZdroje
| - Journal of Thermal Analysis and Calorimetry
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http://linked.open...in/vavai/riv/obor
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http://linked.open...ichTvurcuVysledku
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http://linked.open...cetTvurcuVysledku
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http://linked.open...UplatneniVysledku
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http://linked.open...v/svazekPeriodika
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http://linked.open...iv/tvurceVysledku
| - Dohnalová, Žaneta
- Mikulášek, Petr
- Šulcová, Petra
- Večeřa, Jan
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http://linked.open...ain/vavai/riv/wos
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issn
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number of pages
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http://bibframe.org/vocab/doi
| - 10.1007/s10973-013-3606-1
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http://localhost/t...ganizacniJednotka
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