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  • For reduced titanate nanotubes is necessary to use inert reduction agents for nanotubes. This was the main objective for preparation of reduced titanate nanotubes by low valence of titanium compound. Sodium dititanate was prepared by hydrothermal exfoliation of titanium oxide nanoparticles at concentrated hydroxide sodium environment. Hydrogenated titanate nanotubes was created by ion exchange reaction of sodium salt titanate nanotubes with hydrochloric acid. Reduced titanate nanotubes was prepared by solid state reduction of titanate nanotubes by reaction with low valence of titanium compounds.Thermal stability and reoxidation of low valence titanium componuds was analyzed by thermal analysis (DSC/DTA). Phase and structure of nanotubes was determined by roentgen diffraction (XRD). Nanomorphology of nanotubes was displayed by transmission electron and atomic microscopy (TEM, AFM).
  • For reduced titanate nanotubes is necessary to use inert reduction agents for nanotubes. This was the main objective for preparation of reduced titanate nanotubes by low valence of titanium compound. Sodium dititanate was prepared by hydrothermal exfoliation of titanium oxide nanoparticles at concentrated hydroxide sodium environment. Hydrogenated titanate nanotubes was created by ion exchange reaction of sodium salt titanate nanotubes with hydrochloric acid. Reduced titanate nanotubes was prepared by solid state reduction of titanate nanotubes by reaction with low valence of titanium compounds.Thermal stability and reoxidation of low valence titanium componuds was analyzed by thermal analysis (DSC/DTA). Phase and structure of nanotubes was determined by roentgen diffraction (XRD). Nanomorphology of nanotubes was displayed by transmission electron and atomic microscopy (TEM, AFM). (en)
Title
  • Preparation of reduced titanate nanotubes
  • Preparation of reduced titanate nanotubes (en)
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  • Preparation of reduced titanate nanotubes
  • Preparation of reduced titanate nanotubes (en)
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  • RIV/00216275:25310/13:39896937!RIV14-MSM-25310___
http://linked.open...avai/riv/aktivita
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  • 98998
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  • RIV/00216275:25310/13:39896937
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  • solid state reaction; sonolysis; low valence titanium compound; reduction; titanate nanotubes (en)
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  • [49BA12042F4E]
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  • Pardubice
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  • Conference Proceedings CCT 2013
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  • Kalenda, Petr
  • Kalendová, Andréa
  • Kváča, Zdeněk
  • Mohyla, Martin
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  • Univerzita Pardubice
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  • 978-80-7395-627-1
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  • 25310
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