About: Effect of the Synthesis Conditions on the Formation of MgSrP2O7 and its Characterisation for Pigmentary Application     Goto   Sponge   NotDistinct   Permalink

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  • In present research, we examined MgSrP2O7 as a new pigment with focus on its application as a corrosion inhibitor. The influence of the synthesis conditions on the product properties was examined. Samples were obtained by solid-state reaction and various homogenisation methods of initial components were employed (hand-milling, wet (ethanol/acetone) ball-milling and coprecipitation). Thermal behaviour of the reaction mixtures or dried coprecipitate was investigated using differential thermal and thermo-gravimetric analyses. Obtained samples were characterised with X-ray diffraction analysis, scanning electron microscopy and IR spectroscopy. Focusing on pigmentary application, specific properties of the samples were evaluated, such as thermal stability, mean particle size values and colour parameters, and also preliminary anticorrosion tests have been performed. Based on obtained results, MgSrP2O7 could be considered as a perspective corrosion inhibitor and homogenisation via coprecipitation can be rated as the best method of preparation of this composition, which provides the best thermal stability, the lowest particle size, the best homogeneity and the most promising corrosion inhibition characteristics (pH and rho of the pigment aqua suspension) for the final product.
  • In present research, we examined MgSrP2O7 as a new pigment with focus on its application as a corrosion inhibitor. The influence of the synthesis conditions on the product properties was examined. Samples were obtained by solid-state reaction and various homogenisation methods of initial components were employed (hand-milling, wet (ethanol/acetone) ball-milling and coprecipitation). Thermal behaviour of the reaction mixtures or dried coprecipitate was investigated using differential thermal and thermo-gravimetric analyses. Obtained samples were characterised with X-ray diffraction analysis, scanning electron microscopy and IR spectroscopy. Focusing on pigmentary application, specific properties of the samples were evaluated, such as thermal stability, mean particle size values and colour parameters, and also preliminary anticorrosion tests have been performed. Based on obtained results, MgSrP2O7 could be considered as a perspective corrosion inhibitor and homogenisation via coprecipitation can be rated as the best method of preparation of this composition, which provides the best thermal stability, the lowest particle size, the best homogeneity and the most promising corrosion inhibition characteristics (pH and rho of the pigment aqua suspension) for the final product. (en)
Title
  • Effect of the Synthesis Conditions on the Formation of MgSrP2O7 and its Characterisation for Pigmentary Application
  • Effect of the Synthesis Conditions on the Formation of MgSrP2O7 and its Characterisation for Pigmentary Application (en)
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  • Effect of the Synthesis Conditions on the Formation of MgSrP2O7 and its Characterisation for Pigmentary Application
  • Effect of the Synthesis Conditions on the Formation of MgSrP2O7 and its Characterisation for Pigmentary Application (en)
skos:notation
  • RIV/00216275:25310/13:39896284!RIV14-MSM-25310___
http://linked.open...avai/riv/aktivita
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  • P(EE2.3.30.0021)
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  • 1
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  • 71807
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  • RIV/00216275:25310/13:39896284
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  • Corrosion Test; Solid-State Reaction; Environmentally Friendly Corrosion Inhibition Pigment; Pyrophosphate (en)
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  • NL - Nizozemsko
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  • [7D3924A9F6E9]
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  • Journal of Thermal Analysis and Calorimetry
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  • 113
http://linked.open...iv/tvurceVysledku
  • Dohnalová, Žaneta
  • Šulcová, Petra
  • Gorodylova, Nataliia Oleksandrivna
http://linked.open...ain/vavai/riv/wos
  • 000321567800018
issn
  • 1388-6150
number of pages
http://bibframe.org/vocab/doi
  • 10.1007/s10973-012-2884-3
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  • 25310
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