About: Synthesis and Structure of NCN-Chelated Organobismuth(III) Bis-Pentasulfide     Goto   Sponge   NotDistinct   Permalink

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  • Organobismuth(III) sulfide (1) containing the NCN pincer type chelating ligand L {L = [2, 6-(CH2NMe2)2C6H3]} reacts with one molar equivalent of elemental sulfur to give the unprecedented cyclic bis-pentasulfide LBi(mu-S5)2BiL (2) with the central twelve-membered ring Bi2S10. Compound 2 was obtained as stable orange crystals and was characterized by the help of elemental analysis, X-ray diffraction technique, IR, and Raman spectroscopy.
  • Organobismuth(III) sulfide (1) containing the NCN pincer type chelating ligand L {L = [2, 6-(CH2NMe2)2C6H3]} reacts with one molar equivalent of elemental sulfur to give the unprecedented cyclic bis-pentasulfide LBi(mu-S5)2BiL (2) with the central twelve-membered ring Bi2S10. Compound 2 was obtained as stable orange crystals and was characterized by the help of elemental analysis, X-ray diffraction technique, IR, and Raman spectroscopy. (en)
Title
  • Synthesis and Structure of NCN-Chelated Organobismuth(III) Bis-Pentasulfide
  • Synthesis and Structure of NCN-Chelated Organobismuth(III) Bis-Pentasulfide (en)
skos:prefLabel
  • Synthesis and Structure of NCN-Chelated Organobismuth(III) Bis-Pentasulfide
  • Synthesis and Structure of NCN-Chelated Organobismuth(III) Bis-Pentasulfide (en)
skos:notation
  • RIV/00216275:25310/12:39895565!RIV13-GA0-25310___
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  • I, P(GAP207/10/0130)
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  • 3-4
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  • 172942
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  • RIV/00216275:25310/12:39895565
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  • X-ray diffraction; ring expansion; chelates; sulfur; bismuth; sulfides; germanium; reactivity; chalcogenides; complexes; containing cyclic polysulfides; kinetically stabilized silanethione; bond covalent radii (en)
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  • DE - Spolková republika Německo
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  • [2E2B65B999B3]
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  • Zeitschrift für anorganische und allgemeine Chemie
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  • 638
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  • Dostál, Libor
  • Erben, Milan
  • Jambor, Roman
  • Růžička, Aleš
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  • 000301783500018
issn
  • 0044-2313
number of pages
http://bibframe.org/vocab/doi
  • 10.1002/zaac.201100515
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  • 25310
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