About: Determination of Hexamine in the Dithane DG Fungicide by Using Capillary Isotachophoresis

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	In this article, hexamine (HX; syn.: urotropine, chem.: 1,3,5,7- tetraaza-tricyclo [3.3.1.13,7]decane, C6H12N4) is the analyte of interest determined in commercially marketed fungicide (Dithane DG) with the aid of capillary isotachophoresis. After method development, the optimal electrolyte system comprised 0.01 M KOH + 0.02 M CH3COOH + 0.1 % hydroxyethyl cellulose (pH 4.75) as the leading electrolyte and 0.01 M CH3COOH as the terminator. The calibration / detection characteristics are as follows: linearity over the concentration range of 0-200 mg l-1 HX, limit of detection ca. 2 mg l-1, limit of quantification of ca. 6 mg l-1 HX. Furthermore, relatively simple procedure (involving extraction as the only major sample pretreatment), low operational costs, and sufficient sensitivity are also typical attributes of the method that can be recommended for determination of hexamine in herbicides and related samples. In this article, hexamine (HX; syn.: urotropine, chem.: 1,3,5,7- tetraaza-tricyclo [3.3.1.13,7]decane, C6H12N4) is the analyte of interest determined in commercially marketed fungicide (Dithane DG) with the aid of capillary isotachophoresis. After method development, the optimal electrolyte system comprised 0.01 M KOH + 0.02 M CH3COOH + 0.1 % hydroxyethyl cellulose (pH 4.75) as the leading electrolyte and 0.01 M CH3COOH as the terminator. The calibration / detection characteristics are as follows: linearity over the concentration range of 0-200 mg l-1 HX, limit of detection ca. 2 mg l-1, limit of quantification of ca. 6 mg l-1 HX. Furthermore, relatively simple procedure (involving extraction as the only major sample pretreatment), low operational costs, and sufficient sensitivity are also typical attributes of the method that can be recommended for determination of hexamine in herbicides and related samples. (en)
Title	Determination of Hexamine in the Dithane DG Fungicide by Using Capillary Isotachophoresis Determination of Hexamine in the Dithane DG Fungicide by Using Capillary Isotachophoresis (en)
skos:prefLabel	Determination of Hexamine in the Dithane DG Fungicide by Using Capillary Isotachophoresis Determination of Hexamine in the Dithane DG Fungicide by Using Capillary Isotachophoresis (en)
skos:notation	RIV/00216275:25310/11:39892685!RIV12-MSM-25310___
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(LC06035), Z(MSM0021627502)
http://linked.open...vai/riv/dodaniDat	2012
http://linked.open...aciTvurceVysledku	Švancara, Ivan Bartoš, Martin Martinková, Zdeňka Mikysek, Tomáš
http://linked.open.../riv/druhVysledku	D - Článek ve sborníku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Univerzita Pardubice / Fakulta chemicko-technologická
http://linked.open...dnocenehoVysledku	193833
http://linked.open...ai/riv/idVysledku	RIV/00216275:25310/11:39892685
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	Determination; Capillary isotachophoresis, Hexamine (urotropine), Dithane DG fungicide (en)
http://linked.open.../riv/klicoveSlovo	Capillary isotachophoresis Determination Dithane DG fungicide Hexamine (urotropine)
http://linked.open...ontrolniKodProRIV	[D678994F708C]
http://linked.open...v/mistoKonaniAkce	Pardubice
http://linked.open...i/riv/mistoVydani	Pardubice
http://linked.open...i/riv/nazevZdroje	Sensing in Electroanalysis Vol. 6
http://linked.open...in/vavai/riv/obor	CG
http://linked.open...ichTvurcuVysledku	4 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...vavai/riv/projekt	Centre of Biophysical Chemistry, Bioelectrochemistry and Bioanalysis. New Tools for Genomics, Proteomics and Biomedicine.
http://linked.open...UplatneniVysledku	2011
http://linked.open...iv/tvurceVysledku	Švancara, Ivan Bartoš, Martin Martinková, Zdeňka Mikysek, Tomáš
http://linked.open...vavai/riv/typAkce	EUR - Evropská
http://linked.open.../riv/zahajeniAkce	2011-11-14 (xsd:date)
http://linked.open...n/vavai/riv/zamer	Pokročilé analytické a separační metody a jejich aplikace v diagnostice a technologii živých a neživých materiálů
number of pages	14 (xsd:int)
http://purl.org/ne...btex#hasPublisher	Univerzita Pardubice
https://schema.org/isbn	978-80-7395-434-5
http://localhost/t...ganizacniJednotka	25310

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