About: Reductive amination of Cyclopentanone     Goto   Sponge   NotDistinct   Permalink

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  • Kinetika heterogenní katalytické reduktivní aminace cyklopentanonu byla studována na poloprovozním aktoklávu PAAR. N-cyklopentyliminocykolopentanon byl detekován jako hlavní intermediate v reakční směsi. Bylo zjištěno, že za daných podmínek nevzniká z hlavního intermediátu nežádoucí N,N-dicykopentylamin ale tento podléhá pomalé hydrolýze a vzniká žádaný cyklopentylamin v dobrém výtěžku. Bala zíksána malá množství vedlejších látek jako cyklopentanol a N,N-dicyklopentylamin. Experimentální data byla konfrontována s navrženým kinetickým modelem. (cs)
  • The kinetics of heterogeneous catalytic reductive amination of cyclopentanone has been studied on a pilot plant PARR autoclave. N-cyclopentyliminocyclopentane was detected as the main intermediate in a reaction mixture. It was found that, at the given conditions, the main intermediate does not form the undesirable N,N-dicyclopentylamine but undergoes slow hydrolysis, and the desired product, cyclopentylamine, results in a good yield. Slight amounts of by-products such as cyclopentanole and N,N-dicyclopentylamine were obtained. The experimental data were confronted with the suggested kinetic model.
  • The kinetics of heterogeneous catalytic reductive amination of cyclopentanone has been studied on a pilot plant PARR autoclave. N-cyclopentyliminocyclopentane was detected as the main intermediate in a reaction mixture. It was found that, at the given conditions, the main intermediate does not form the undesirable N,N-dicyclopentylamine but undergoes slow hydrolysis, and the desired product, cyclopentylamine, results in a good yield. Slight amounts of by-products such as cyclopentanole and N,N-dicyclopentylamine were obtained. The experimental data were confronted with the suggested kinetic model. (en)
Title
  • Reductive amination of Cyclopentanone
  • Reductive amination of Cyclopentanone (en)
  • Reduktivní aminace cyklopentanonu (cs)
skos:prefLabel
  • Reductive amination of Cyclopentanone
  • Reductive amination of Cyclopentanone (en)
  • Reduktivní aminace cyklopentanonu (cs)
skos:notation
  • RIV/00216275:25310/05:00002684!RIV08-MSM-25310___
http://linked.open.../vavai/riv/strany
  • 202-210
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM0021627501)
http://linked.open...iv/cisloPeriodika
  • 2
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 540409
http://linked.open...ai/riv/idVysledku
  • RIV/00216275:25310/05:00002684
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Cyclopentanone; Cyclopentylamine; N-cyclopentyliminocyclopentane; Heterogeneous catalytic reductive amination; Kinetics (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV
  • [968A9F54B34D]
http://linked.open...i/riv/nazevZdroje
  • Applied catalysis A-General
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 286
http://linked.open...iv/tvurceVysledku
  • Doležal, Petr
  • Hrdina, Radim
  • Pavelek, Martin
  • Machalický, Oldřich
  • Šuláková, Romana
  • Hrádková, Květoslava
  • Kubec, Petr
http://linked.open...n/vavai/riv/zamer
issn
  • 0926-860X
number of pages
http://localhost/t...ganizacniJednotka
  • 25310
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