About: Determination of the Interdetector Volume by s-detection in Size-Exclusion Chromatography of Polymers with on-line Multiangle Light-Scattering Detection

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About: Determination of the Interdetector Volume by s-detection in Size-Exclusion Chromatography of Polymers with on-line Multiangle Light-Scattering Detection Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Byl stanoven interdetektorový objem při SEC chromatografii polymerů při použití MALS/koncentrační detektoru. (cs) The determination of the interdetector volume (IDV) in size-exclusion chromatography (SEC) of polymers with dual multiangle light-scattering/concentration detection based on the s-detection is demonstrated. By s-detection the determination is meant of local molecular mass from a known relation between molecular mass and radius of gyration, obtained from the angle dependence of the intensity of scattered light. IDV is found basing on the stipulation of equal slope of local calibrations found by the dual light-scattering/concentration detection, referred to as the w- and s-detection. As the s-detection uses just the light-scattering detector and, therefore, is independent of the value of IDV, this quantity can be found by searching for its value that gives the local calibration dependence obtained by the dual detection closest to that determined independently by the s-detection. The determination of the interdetector volume (IDV) in size-exclusion chromatography (SEC) of polymers with dual multiangle light-scattering/concentration detection based on the s-detection is demonstrated. By s-detection the determination is meant of local molecular mass from a known relation between molecular mass and radius of gyration, obtained from the angle dependence of the intensity of scattered light. IDV is found basing on the stipulation of equal slope of local calibrations found by the dual light-scattering/concentration detection, referred to as the w- and s-detection. As the s-detection uses just the light-scattering detector and, therefore, is independent of the value of IDV, this quantity can be found by searching for its value that gives the local calibration dependence obtained by the dual detection closest to that determined independently by the s-detection. (en)
Title	Stanovení mezidetektorového objemu při SEC analýze polymerů (cs) Determination of the Interdetector Volume by s-detection in Size-Exclusion Chromatography of Polymers with on-line Multiangle Light-Scattering Detection Determination of the Interdetector Volume by s-detection in Size-Exclusion Chromatography of Polymers with on-line Multiangle Light-Scattering Detection (en)
skos:prefLabel	Stanovení mezidetektorového objemu při SEC analýze polymerů (cs) Determination of the Interdetector Volume by s-detection in Size-Exclusion Chromatography of Polymers with on-line Multiangle Light-Scattering Detection Determination of the Interdetector Volume by s-detection in Size-Exclusion Chromatography of Polymers with on-line Multiangle Light-Scattering Detection (en)
skos:notation	RIV/00216275:25310/04:00001534!RIV08-MSM-25310___
http://linked.open.../vavai/riv/strany	37-41
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(KSK4050111), Z(MSM 253100001)
http://linked.open...iv/cisloPeriodika	1-2
http://linked.open...vai/riv/dodaniDat	2008
http://linked.open...aciTvurceVysledku	Podzimek, Štěpán
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Univerzita Pardubice / Fakulta chemicko-technologická
http://linked.open...dnocenehoVysledku	560123
http://linked.open...ai/riv/idVysledku	RIV/00216275:25310/04:00001534
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	detection; LC; multiangle light scattering detection; interdetector volume; radius of gyration; peak broadening; polymers (en)
http://linked.open.../riv/klicoveSlovo	multiangle light scattering detection polymers LC peak broadening detection radius of gyration interdetector volume
http://linked.open...odStatuVydavatele	NL - Nizozemsko
http://linked.open...ontrolniKodProRIV	[7D7E5B03D879]
http://linked.open...i/riv/nazevZdroje	Journal of Chromatography A
http://linked.open...in/vavai/riv/obor	CB
http://linked.open...ichTvurcuVysledku	1 (xsd:int)
http://linked.open...cetTvurcuVysledku	3 (xsd:int)
http://linked.open...vavai/riv/projekt	Goal-oriented preparation of chemical compounds with well-defined properties
http://linked.open...UplatneniVysledku	2004
http://linked.open...v/svazekPeriodika	1045
http://linked.open...iv/tvurceVysledku	Podzimek, Štěpán Kratochvíl, Pavel Netopilík, Miroslav
http://linked.open...n/vavai/riv/zamer	http://linked.opendata.cz/resource/domain/vavai/zamer/MSM%20253100001
issn	0021-9673
number of pages	5 (xsd:int)
http://localhost/t...ganizacniJednotka	25310

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