About: Rapid Determination of Lead in Submicroliter Samples of Whole Blood using Diode Laser Thermal Vaporization     Goto   Sponge   NotDistinct   Permalink

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  • A method for determination of trace elements in submicroliter sample volumes, diode laser thermal vaporization (DLTV) inductively-coupled plasma mass spectrometry (ICP-MS) is presented. Analyte is desorbed from a substrate, such as paper or cellulose containing a suitable absorber, using a continuous-wave diode laser. The laser induces pyrolysis of the substrate and the generated aerosol is carried out into the plasma torch. Unlike laser ablation, DLTV does not require an expensive high-energy pulse laser, which makes it a promising alternative to nebulizers. Analysis of lead in whole blood is demonstrated. Advantages of the method, simplicity, speed, easy archiving and transportation of samples and low cost, are presented. Selection of experimental arrangement and laser wavelength as well as optimization of experimental conditions, e.g., raster type, scan speed, additives etc. was examined.
  • A method for determination of trace elements in submicroliter sample volumes, diode laser thermal vaporization (DLTV) inductively-coupled plasma mass spectrometry (ICP-MS) is presented. Analyte is desorbed from a substrate, such as paper or cellulose containing a suitable absorber, using a continuous-wave diode laser. The laser induces pyrolysis of the substrate and the generated aerosol is carried out into the plasma torch. Unlike laser ablation, DLTV does not require an expensive high-energy pulse laser, which makes it a promising alternative to nebulizers. Analysis of lead in whole blood is demonstrated. Advantages of the method, simplicity, speed, easy archiving and transportation of samples and low cost, are presented. Selection of experimental arrangement and laser wavelength as well as optimization of experimental conditions, e.g., raster type, scan speed, additives etc. was examined. (en)
Title
  • Rapid Determination of Lead in Submicroliter Samples of Whole Blood using Diode Laser Thermal Vaporization
  • Rapid Determination of Lead in Submicroliter Samples of Whole Blood using Diode Laser Thermal Vaporization (en)
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  • Rapid Determination of Lead in Submicroliter Samples of Whole Blood using Diode Laser Thermal Vaporization
  • Rapid Determination of Lead in Submicroliter Samples of Whole Blood using Diode Laser Thermal Vaporization (en)
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  • RIV/00216224:14740/12:00057420!RIV13-GA0-14740___
http://linked.open...avai/riv/aktivita
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  • P(ED1.1.00/02.0068), P(GAP206/12/0538), S
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  • 164093
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  • RIV/00216224:14740/12:00057420
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  • lead; blood; laser diode; thermal vaporization; inductively coupled plasma; mass spectrometry; LDTV (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...ontrolniKodProRIV
  • [09211E73AB3B]
http://linked.open...in/vavai/riv/obor
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  • Kanický, Viktor
  • Preisler, Jan
  • Foltynová, Pavla
http://localhost/t...ganizacniJednotka
  • 14740
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