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  • This study deals with the nonaqueous capillary electrophoretic separation of dextromethorphan and its metabolites using a methanolic background electrolyte. The optimization of separation conditions was performed in terms of the resolution of dextromethorphan and dextrorphan and the effect of separation temperature, voltage, and the characteristics of the background electrolyte were studied. Complete separation of all analytes was achieved in 40 mM ammonium acetate dissolved in methanol. Hydrodynamic injection was performed at 3 kPa for 4 s. The separation voltage was 20 kV accompanied by a low electric current. The ultraviolet detection was performed at 214 nm, the temperature of the capillary was 25°C. These conditions enabled the separation of four analytes plus the internal standard within 9 min. Further, the developed method was validated in terms of linearity, sensitivity, and repeatability.
  • This study deals with the nonaqueous capillary electrophoretic separation of dextromethorphan and its metabolites using a methanolic background electrolyte. The optimization of separation conditions was performed in terms of the resolution of dextromethorphan and dextrorphan and the effect of separation temperature, voltage, and the characteristics of the background electrolyte were studied. Complete separation of all analytes was achieved in 40 mM ammonium acetate dissolved in methanol. Hydrodynamic injection was performed at 3 kPa for 4 s. The separation voltage was 20 kV accompanied by a low electric current. The ultraviolet detection was performed at 214 nm, the temperature of the capillary was 25°C. These conditions enabled the separation of four analytes plus the internal standard within 9 min. Further, the developed method was validated in terms of linearity, sensitivity, and repeatability. (en)
Title
  • Nonaqueous capillary electrophoresis of dextromethorphan and its metabolites
  • Nonaqueous capillary electrophoresis of dextromethorphan and its metabolites (en)
skos:prefLabel
  • Nonaqueous capillary electrophoresis of dextromethorphan and its metabolites
  • Nonaqueous capillary electrophoresis of dextromethorphan and its metabolites (en)
skos:notation
  • RIV/00216224:14310/14:00074172!RIV15-GA0-14310___
http://linked.open...avai/riv/aktivita
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  • P(GBP206/12/G014)
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  • 19
http://linked.open...vai/riv/dodaniDat
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  • 32719
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  • RIV/00216224:14310/14:00074172
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  • Dextromethorphan; Dextrorphan; Methanol; Nonaqueous media (en)
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  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [E8A049905A80]
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  • JOURNAL OF SEPARATION SCIENCE
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  • 37
http://linked.open...iv/tvurceVysledku
  • Juřica, Jan
  • Glatz, Zdeněk
  • Langmajerová, Monika
  • Cvingráfová, Eliška
  • Pelcová, Marta
http://linked.open...ain/vavai/riv/wos
  • 000342909300021
issn
  • 1615-9306
number of pages
http://bibframe.org/vocab/doi
  • 10.1002/jssc.201400582
http://localhost/t...ganizacniJednotka
  • 14310
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