About: Determination of carbon in solidified sodium coolant usingnew ICP-OES methods

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About: Determination of carbon in solidified sodium coolant usingnew ICP-OES methods Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	New methods for the determination of carbon in sodium using laser ablation inductively coupled plasma optical emission spectrometry (LA-ICP-OES) and ICP-OES with pneumatic nebulisation (PN-ICP-OES) were developed. The determination was required for the study of the carbon dioxide reaction with molten sodium at high temperatures (300–600C). After exposition to CO2, the solidified sodium sample was subjected to direct solid analysis by LA-ICP-OES and to solution analysis. For the determination of carbon in the sodium sample surface layer by LA-ICP-OES, three different matrices containing sodium were tested (NaCl, NaF, and Na2B4O7 10H2O) as calibration pellets. The calibration dependences were improved using sodium as the internal standard. Average carbon content in the sodium bulk sample was determined by PN-ICP-OES after the sample dissolution by water vapour. New methods for the determination of carbon in sodium using laser ablation inductively coupled plasma optical emission spectrometry (LA-ICP-OES) and ICP-OES with pneumatic nebulisation (PN-ICP-OES) were developed. The determination was required for the study of the carbon dioxide reaction with molten sodium at high temperatures (300–600C). After exposition to CO2, the solidified sodium sample was subjected to direct solid analysis by LA-ICP-OES and to solution analysis. For the determination of carbon in the sodium sample surface layer by LA-ICP-OES, three different matrices containing sodium were tested (NaCl, NaF, and Na2B4O7 10H2O) as calibration pellets. The calibration dependences were improved using sodium as the internal standard. Average carbon content in the sodium bulk sample was determined by PN-ICP-OES after the sample dissolution by water vapour. (en)
Title	Determination of carbon in solidified sodium coolant usingnew ICP-OES methods Determination of carbon in solidified sodium coolant usingnew ICP-OES methods (en)
skos:prefLabel	Determination of carbon in solidified sodium coolant usingnew ICP-OES methods Determination of carbon in solidified sodium coolant usingnew ICP-OES methods (en)
skos:notation	RIV/00216224:14310/11:00050724!RIV12-MPO-14310___
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(2A-1TP1/067), Z(MSM0021622410), Z(MSM0021622411)
http://linked.open...iv/cisloPeriodika	5
http://linked.open...vai/riv/dodaniDat	2012
http://linked.open...aciTvurceVysledku	Otruba, Vítězslav Vaculovič, Tomáš Kanický, Viktor
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Masarykova univerzita / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	193812
http://linked.open...ai/riv/idVysledku	RIV/00216224:14310/11:00050724
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	ICP-OES; laser ablation; molten sodium (en)
http://linked.open.../riv/klicoveSlovo	ICP-OES molten sodium laser ablation
http://linked.open...odStatuVydavatele	PL - Polská republika
http://linked.open...ontrolniKodProRIV	[5CDBEA1E8007]
http://linked.open...i/riv/nazevZdroje	Chemical Papers
http://linked.open...in/vavai/riv/obor	CB
http://linked.open...ichTvurcuVysledku	3 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...vavai/riv/projekt	Research into technologies for high potentional heat transfer from a nuclear source
http://linked.open...UplatneniVysledku	2011
http://linked.open...v/svazekPeriodika	65
http://linked.open...iv/tvurceVysledku	Kanický, Viktor Matal, Oldřich Otruba, Vítězslav Vaculovič, Tomáš
http://linked.open...n/vavai/riv/zamer	Study and application of plasma chemical reactions in non-isothermic low temperature plasma and its interaction with solid surface Physical and chemical properties of advanced materials and structures
issn	0366-6352
number of pages	6 (xsd:int)
http://localhost/t...ganizacniJednotka	14310

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