About: Synthesis, structure and thermal decomposition of [Ni(NH3)(6)][VO(O-2)(2)(NH3)](2)     Goto   Sponge   NotDistinct   Permalink

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Description
  • The compound [Ni(NH3)(6)][VO(O-2)(2)(NH3)](2) was prepared and characterized by elemental analysis and vibrational spectra. The single crystal X-ray study revealed that the structure consists of [Ni(NH3)(6)](2+) and [VO(O-2)(2)(NH3)]- ions. As a result of weak interionic interactions V'... O-p(O-p-peroxo oxygen), ([VO(O-2)(2)(NH3)])(2) dimers are formed in the solid-state. The thermal decomposition of [Ni(NH3)(6)][VO(O-2)(2)(NH3)](2) is a multi-step process with overlapped individual steps; no defined intermediates were obtained. The final solid products of thermal decomposition up to 600C were Ni2V2O7 and V2O5.
  • The compound [Ni(NH3)(6)][VO(O-2)(2)(NH3)](2) was prepared and characterized by elemental analysis and vibrational spectra. The single crystal X-ray study revealed that the structure consists of [Ni(NH3)(6)](2+) and [VO(O-2)(2)(NH3)]- ions. As a result of weak interionic interactions V'... O-p(O-p-peroxo oxygen), ([VO(O-2)(2)(NH3)])(2) dimers are formed in the solid-state. The thermal decomposition of [Ni(NH3)(6)][VO(O-2)(2)(NH3)](2) is a multi-step process with overlapped individual steps; no defined intermediates were obtained. The final solid products of thermal decomposition up to 600C were Ni2V2O7 and V2O5. (en)
Title
  • Synthesis, structure and thermal decomposition of [Ni(NH3)(6)][VO(O-2)(2)(NH3)](2)
  • Synthesis, structure and thermal decomposition of [Ni(NH3)(6)][VO(O-2)(2)(NH3)](2) (en)
skos:prefLabel
  • Synthesis, structure and thermal decomposition of [Ni(NH3)(6)][VO(O-2)(2)(NH3)](2)
  • Synthesis, structure and thermal decomposition of [Ni(NH3)(6)][VO(O-2)(2)(NH3)](2) (en)
skos:notation
  • RIV/00216224:14310/08:00026159!RIV10-MSM-14310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM0021622415)
http://linked.open...iv/cisloPeriodika
  • 1
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
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  • 398817
http://linked.open...ai/riv/idVysledku
  • RIV/00216224:14310/08:00026159
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • ammine complexes; IR spectra; thermal decomposition; X-ray structure (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [2A1EEDEE70DC]
http://linked.open...i/riv/nazevZdroje
  • Journal of Thermal Analysis
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 91
http://linked.open...iv/tvurceVysledku
  • Marek, Jaromír
  • Schwendt, P.
  • Drábik, M.
  • Chrappová, J.
  • Dudášová, D.
http://linked.open...ain/vavai/riv/wos
  • 000252889200044
http://linked.open...n/vavai/riv/zamer
issn
  • 1388-6150
number of pages
http://localhost/t...ganizacniJednotka
  • 14310
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