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  • In this paper, the sol gel synthesis and characteristic properties of kalsilite type alumosilicates (KAlSiO4 and K0.5Na0.5AlSiO4) are reported. The polycrystalline powders were characterized by thermal analysis (TG/DTA), powder X ray diffraction analysis (XRD) and scanning electron microscopy (SEM). Single phase kalsilite oxides have been obtained after annealing precursor gels for 5 h in the temperature range of 750 to 850 C. It was demonstrated that crystallinity of the samples slightly depends on the temperature of annealing. From the results obtained, it could be concluded that the KAlSiO4 solids are composed of the volumetric plate like grains with no regular size (from 5 to 30 microm at 750 C and around 5 to 50 microm at 850 C). Larger crystallites for mixed potassium sodium kalsilite have formed (from 10 to 80 microm at 750 C and above 100 microm at 850 C) in comparison with potassium kalsilite samples).
  • In this paper, the sol gel synthesis and characteristic properties of kalsilite type alumosilicates (KAlSiO4 and K0.5Na0.5AlSiO4) are reported. The polycrystalline powders were characterized by thermal analysis (TG/DTA), powder X ray diffraction analysis (XRD) and scanning electron microscopy (SEM). Single phase kalsilite oxides have been obtained after annealing precursor gels for 5 h in the temperature range of 750 to 850 C. It was demonstrated that crystallinity of the samples slightly depends on the temperature of annealing. From the results obtained, it could be concluded that the KAlSiO4 solids are composed of the volumetric plate like grains with no regular size (from 5 to 30 microm at 750 C and around 5 to 50 microm at 850 C). Larger crystallites for mixed potassium sodium kalsilite have formed (from 10 to 80 microm at 750 C and above 100 microm at 850 C) in comparison with potassium kalsilite samples). (en)
Title
  • Study of alumosilicate porcelains: Sol-gel preparation, characterization and erosion evaluated by gravimetric method
  • Study of alumosilicate porcelains: Sol-gel preparation, characterization and erosion evaluated by gravimetric method (en)
skos:prefLabel
  • Study of alumosilicate porcelains: Sol-gel preparation, characterization and erosion evaluated by gravimetric method
  • Study of alumosilicate porcelains: Sol-gel preparation, characterization and erosion evaluated by gravimetric method (en)
skos:notation
  • RIV/00216224:14310/08:00024933!RIV11-GA0-14310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA203/04/0296), Z(MSM0021622410)
http://linked.open...iv/cisloPeriodika
  • 11
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 398083
http://linked.open...ai/riv/idVysledku
  • RIV/00216224:14310/08:00024933
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • Ceramics; Inorganic compounds; Oxides; Sol-gel chemistry (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [E62DC266A37C]
http://linked.open...i/riv/nazevZdroje
  • Materials Research Bulletin
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 43
http://linked.open...iv/tvurceVysledku
  • Pinkas, Jiří
  • Kareiva, Aivaras
  • Beganskiene, Aldona
  • Bogdanoviciene, Irma
  • Jankeviciute, Audrone
http://linked.open...ain/vavai/riv/wos
  • 000260292400021
http://linked.open...n/vavai/riv/zamer
issn
  • 0025-5408
number of pages
http://localhost/t...ganizacniJednotka
  • 14310
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