About: Analysis of Thiocyanate in Biological Fluids by Capillary Zone Electrophoresis

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	A new sensitive and simple method has been developed for the determination of thiocyanate in human serum, urine and saliva. The determinations were performed in a 75 mm fused silica capillary (64.5 cm length, 56 cm effective length) using 0.1 M b-alanine - HCl (pH 3.50) as a background electrolyte, separation voltage 18 kV (negative polarity), temperature of capillary 25 oC and direct detection at 200 nm. Serum samples were 10-times diluted with deionised water and deproteinised with acetonitrile in the ratio 1 : 2. Urine and saliva samples need only 20-fold dilution with deionised water. The proposed method was successfully applied to the determination of thiocyanate in various human serum, saliva and urine samples. A new sensitive and simple method has been developed for the determination of thiocyanate in human serum, urine and saliva. The determinations were performed in a 75 mm fused silica capillary (64.5 cm length, 56 cm effective length) using 0.1 M b-alanine - HCl (pH 3.50) as a background electrolyte, separation voltage 18 kV (negative polarity), temperature of capillary 25 oC and direct detection at 200 nm. Serum samples were 10-times diluted with deionised water and deproteinised with acetonitrile in the ratio 1 : 2. Urine and saliva samples need only 20-fold dilution with deionised water. The proposed method was successfully applied to the determination of thiocyanate in various human serum, saliva and urine samples. (en) A new sensitive and simple method has been developed for the determination of thiocyanate in human serum, urine and saliva. The determinations were performed in a 75 mm fused silica capillary (64.5 cm length, 56 cm effective length) using 0.1 M b-alanine - HCl (pH 3.50) as a background electrolyte, separation voltage 18 kV (negative polarity), temperature of capillary 25 oC and direct detection at 200 nm. Serum samples were 10-times diluted with deionised water and deproteinised with acetonitrile in the ratio 1 : 2. Urine and saliva samples need only 20-fold dilution with deionised water. The proposed method was successfully applied to the determination of thiocyanate in various human serum, saliva and urine samples. (cs)
Title	Analysis of Thiocyanate in Biological Fluids by Capillary Zone Electrophoresis Analysis of Thiocyanate in Biological Fluids by Capillary Zone Electrophoresis (en) Analysis of Thiocyanate in Biological Fluids by Capillary Zone Electrophoresis (cs)
skos:prefLabel	Analysis of Thiocyanate in Biological Fluids by Capillary Zone Electrophoresis Analysis of Thiocyanate in Biological Fluids by Capillary Zone Electrophoresis (en) Analysis of Thiocyanate in Biological Fluids by Capillary Zone Electrophoresis (cs)
skos:notation	RIV/00216224:14310/01:00003597!RIV09-GA0-14310___
http://linked.open...avai/riv/aktivita	P
http://linked.open...avai/riv/aktivity	P(GA525/00/0785)
http://linked.open...iv/cisloPeriodika	(1+2)
http://linked.open...vai/riv/dodaniDat	2009
http://linked.open...aciTvurceVysledku	Štěrbová, Hana Vytisková, Soňa Glatz, Zdeněk
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Masarykova univerzita / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	673147
http://linked.open...ai/riv/idVysledku	RIV/00216224:14310/01:00003597
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	Capillary electrophoresis; Rhodenase; Thiocyanate; Biuological Fluids (en)
http://linked.open.../riv/klicoveSlovo	Capillary electrophoresis Thiocyanate Rhodenase Biuological Fluids
http://linked.open...odStatuVydavatele	NL - Nizozemsko
http://linked.open...ontrolniKodProRIV	[B7C885A68991]
http://linked.open...i/riv/nazevZdroje	Journal of Chromatography A
http://linked.open...in/vavai/riv/obor	CE
http://linked.open...ichTvurcuVysledku	3 (xsd:int)
http://linked.open...cetTvurcuVysledku	3 (xsd:int)
http://linked.open...vavai/riv/projekt	Acidification processes in sulphide wastes
http://linked.open...UplatneniVysledku	2001
http://linked.open...v/svazekPeriodika	916
http://linked.open...iv/tvurceVysledku	Glatz, Zdeněk Vytisková, Soňa Štěrbová, Hana
issn	0021-9606
number of pages	5 (xsd:int)
http://localhost/t...ganizacniJednotka	14310

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