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  • The structure of titanate nanotubes (Ti-NTs) was studied by a combination of powder X-ray diffraction (PXRD), electron diffraction and high resolution transmission electron microscopy (HRTEM). Ti-NTs are prepared by hydrothermal treatment of TiO2 powder. The structure is identified by powder X-ray diffraction as the one based on the structure of H2Ti2O5 center dot H2O phase. The same structure is obtained by projected potential from HRTEM through-focus image series. The structure is verified by simulated PXRD pattern with the aid of the Debye formula. The validity of the model is tested by computing Fourier transformation of a single nanotube which is proportional to measured electron diffraction intensities. A good agreement of this calculation with measured precession electron diffraction data is achieved. (C) 2013 Elsevier Inc. All rights reserved.
  • The structure of titanate nanotubes (Ti-NTs) was studied by a combination of powder X-ray diffraction (PXRD), electron diffraction and high resolution transmission electron microscopy (HRTEM). Ti-NTs are prepared by hydrothermal treatment of TiO2 powder. The structure is identified by powder X-ray diffraction as the one based on the structure of H2Ti2O5 center dot H2O phase. The same structure is obtained by projected potential from HRTEM through-focus image series. The structure is verified by simulated PXRD pattern with the aid of the Debye formula. The validity of the model is tested by computing Fourier transformation of a single nanotube which is proportional to measured electron diffraction intensities. A good agreement of this calculation with measured precession electron diffraction data is achieved. (C) 2013 Elsevier Inc. All rights reserved. (en)
Title
  • Study of titanate nanotubes by X-ray and electron diffraction and electron microscopy
  • Study of titanate nanotubes by X-ray and electron diffraction and electron microscopy (en)
skos:prefLabel
  • Study of titanate nanotubes by X-ray and electron diffraction and electron microscopy
  • Study of titanate nanotubes by X-ray and electron diffraction and electron microscopy (en)
skos:notation
  • RIV/00216208:11320/14:10210406!RIV15-MSM-11320___
http://linked.open...avai/riv/aktivita
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  • I, P(GAP108/11/1539), P(LM2011025), S
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  • 48374
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  • RIV/00216208:11320/14:10210406
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  • Debye formula; X-ray powder diffraction; Titanate nanotubes; Electron diffraction; Transmission electron microscopy; Computer simulations (en)
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  • US - Spojené státy americké
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  • [A9B9AED5B6C9]
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  • Materials Characterization
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  • 87
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  • Daniš, Stanislav
  • Kužel, Radomír
  • Brunátová, Tereza
  • Popelková, Daniela
  • Oleynikov, Peter
  • Wan, Wei
  • Zou, Xiaodong
http://linked.open...ain/vavai/riv/wos
  • 000331421600019
issn
  • 1044-5803
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.matchar.2013.11.010
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  • 11320
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