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  • The voltammetric behavior of 5- nitroindazole (5-NI) has been investigated using mercury meniscus modified (m-AgSAE) silver solid amalgam electrode (inner diameter 0.5 mm). Differential pulse voltammetry (DPV) and cyclic voltammetry (CV) were used for study of electrochemical behavior of 5-NI. Britton-Robinson buffer was found to be the best available supporting electrolyte for 5-NI determination. The reaction mechanism was investigated by CV and by elimination voltammetry with linear scan (EVLS). DPV with optimized working parameters was applied for analysis of model solutions containing 5-NI. The limit of detection was calculated as 0.14 uM L for m-AgSAE. Proposed method was successfully tested for analysis of real water samples spiked by 5-NI.
  • The voltammetric behavior of 5- nitroindazole (5-NI) has been investigated using mercury meniscus modified (m-AgSAE) silver solid amalgam electrode (inner diameter 0.5 mm). Differential pulse voltammetry (DPV) and cyclic voltammetry (CV) were used for study of electrochemical behavior of 5-NI. Britton-Robinson buffer was found to be the best available supporting electrolyte for 5-NI determination. The reaction mechanism was investigated by CV and by elimination voltammetry with linear scan (EVLS). DPV with optimized working parameters was applied for analysis of model solutions containing 5-NI. The limit of detection was calculated as 0.14 uM L for m-AgSAE. Proposed method was successfully tested for analysis of real water samples spiked by 5-NI. (en)
Title
  • Use of the Silver Solid Amalgam Electrode for Determination of 5-Nitroindazole
  • Use of the Silver Solid Amalgam Electrode for Determination of 5-Nitroindazole (en)
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  • Use of the Silver Solid Amalgam Electrode for Determination of 5-Nitroindazole
  • Use of the Silver Solid Amalgam Electrode for Determination of 5-Nitroindazole (en)
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  • RIV/00216208:11310/14:10285806!RIV15-MSM-11310___
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  • I, P(GAP208/12/1645)
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  • 52370
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  • RIV/00216208:11310/14:10285806
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  • Elimination voltammetry with linear scan; Voltammetry; Silver solid amalgam electrode; 5-nitroindazole (en)
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  • [4E410609D36C]
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  • Jetřichovice, Czech Republic
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  • Ústí nad Labem
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  • Sborník přednášek mezinárodní odborné konference XXXIV. Moderní Elektrochemické Metody Jetřichovice 19.- 23. května 2014
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  • Barek, Jiří
  • Navrátil, Tomáš
  • Nováková, Kateřina
  • Vyskočil, Vlastimil
  • Chýlková, Jaromíra
  • Hrdlička, Vojtěch
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number of pages
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  • Srsenová Lenka - Best servis Ústí nad Labem
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  • 978-80-905221-2-1
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  • 11310
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