About: Tubular and Microcylindrical Platinum Electrodes for Amperometric Detection of Aminobiphenyls and Aminonaphthalenes in HPLC

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About: Tubular and Microcylindrical Platinum Electrodes for Amperometric Detection of Aminobiphenyls and Aminonaphthalenes in HPLC Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
rdfs:seeAlso	http://dx.doi.org/10.1002/elan.201300579
Description	Platinum electrodes in microcylindrical and tubular arrangements were compared as working electrodes for amperometric detection of 2-aminobiphenyl, 4-aminobiphenyl, 1-aminonaphthalene, and 2-aminonaphthalene in HPLC. Factors influencing separation efficiency are favourable for microcylindrical arrangement while tubular arrangement exhibits higher sensitivities and lower limits of detection. These are in the range of 0.0078-0.027 mu molL(-1) for tubular, and 0.11-0.42 mu molL(-1) for microcylindrical arrangement. Further, a new method with nanomolar detection limits was proposed for determination of tested compounds in urine using solid phase extraction for preliminary separation and preconcentration of the analytes. Platinum electrodes in microcylindrical and tubular arrangements were compared as working electrodes for amperometric detection of 2-aminobiphenyl, 4-aminobiphenyl, 1-aminonaphthalene, and 2-aminonaphthalene in HPLC. Factors influencing separation efficiency are favourable for microcylindrical arrangement while tubular arrangement exhibits higher sensitivities and lower limits of detection. These are in the range of 0.0078-0.027 mu molL(-1) for tubular, and 0.11-0.42 mu molL(-1) for microcylindrical arrangement. Further, a new method with nanomolar detection limits was proposed for determination of tested compounds in urine using solid phase extraction for preliminary separation and preconcentration of the analytes. (en)
Title	Tubular and Microcylindrical Platinum Electrodes for Amperometric Detection of Aminobiphenyls and Aminonaphthalenes in HPLC Tubular and Microcylindrical Platinum Electrodes for Amperometric Detection of Aminobiphenyls and Aminonaphthalenes in HPLC (en)
skos:prefLabel	Tubular and Microcylindrical Platinum Electrodes for Amperometric Detection of Aminobiphenyls and Aminonaphthalenes in HPLC Tubular and Microcylindrical Platinum Electrodes for Amperometric Detection of Aminobiphenyls and Aminonaphthalenes in HPLC (en)
skos:notation	RIV/00216208:11310/14:10218638!RIV15-MSM-11310___
http://linked.open...avai/riv/aktivita	I P S
http://linked.open...avai/riv/aktivity	I, P(GBP206/12/G151), S
http://linked.open...iv/cisloPeriodika	4
http://linked.open...vai/riv/dodaniDat	2015
http://linked.open...aciTvurceVysledku	Pecková, Karolina Zavázalová, Jaroslava Dejmková, Hana Barek, Jiří
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Univerzita Karlova v Praze / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	51380
http://linked.open...ai/riv/idVysledku	RIV/00216208:11310/14:10218638
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	Urine; Solid phase extraction; Platinum electrode; Electrochemical detection; Aminoderivatives of polycyclic aromatic hydrocarbons (en)
http://linked.open.../riv/klicoveSlovo	Urine Electrochemical detection Solid phase extraction Aminoderivatives of polycyclic aromatic hydrocarbons Platinum electrode
http://linked.open...odStatuVydavatele	DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV	[AFB9F63ABD42]
http://linked.open...i/riv/nazevZdroje	Electroanalysis
http://linked.open...in/vavai/riv/obor	CG
http://linked.open...ichTvurcuVysledku	4 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...vavai/riv/projekt	Center of novel approaches to bioanalysis and molecular diagnostics
http://linked.open...UplatneniVysledku	2014
http://linked.open...v/svazekPeriodika	26
http://linked.open...iv/tvurceVysledku	Barek, Jiří Pecková, Karolina Dejmková, Hana Zavázalová, Jaroslava
http://linked.open...ain/vavai/riv/wos	000333749500004
issn	1040-0397
number of pages	10 (xsd:int)
http://bibframe.org/vocab/doi	10.1002/elan.201300579
http://localhost/t...ganizacniJednotka	11310

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