About: Development of a solid-phase extraction with capillary liquid chromatography tandem mass spectrometry for analysis of estrogens in environmental water samples

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About: Development of a solid-phase extraction with capillary liquid chromatography tandem mass spectrometry for analysis of estrogens in environmental water samples Goto Sponge NotDistinct Permalink

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Capillary liquid chromatography (cLC) hyphenated with tandem mass spectrometry (MS-MS) was used to separate and quantitate trace concentrations of five estrogens in aqueous samples. New C-18-based sorption materials bound to the silica support by monomeric and polymeric mechanisms were compared and tested for solid-phase extraction (SPE) of selected analytes with respect to optimization of their preconcentration yield. Application of an endcapped, monomer-bound preconcentration Discovery DSC-18Lt column under the optimized conditions provides yields in the range from 95 to 100% with a high repeatability (n =3, RSD {= 7.2%). Capillary liquid chromatography (cLC) hyphenated with tandem mass spectrometry (MS-MS) was used to separate and quantitate trace concentrations of five estrogens in aqueous samples. New C-18-based sorption materials bound to the silica support by monomeric and polymeric mechanisms were compared and tested for solid-phase extraction (SPE) of selected analytes with respect to optimization of their preconcentration yield. Application of an endcapped, monomer-bound preconcentration Discovery DSC-18Lt column under the optimized conditions provides yields in the range from 95 to 100% with a high repeatability (n =3, RSD {= 7.2%). (en)
Title	Development of a solid-phase extraction with capillary liquid chromatography tandem mass spectrometry for analysis of estrogens in environmental water samples Development of a solid-phase extraction with capillary liquid chromatography tandem mass spectrometry for analysis of estrogens in environmental water samples (en)
skos:prefLabel	Development of a solid-phase extraction with capillary liquid chromatography tandem mass spectrometry for analysis of estrogens in environmental water samples Development of a solid-phase extraction with capillary liquid chromatography tandem mass spectrometry for analysis of estrogens in environmental water samples (en)
skos:notation	RIV/00216208:11310/11:10089764!RIV13-MSM-11310___
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(1M06011), P(7F09016), Z(MSM0021620857)
http://linked.open...iv/cisloPeriodika	15
http://linked.open...vai/riv/dodaniDat	2013
http://linked.open...aciTvurceVysledku	Čabala, Radomír Kozlík, Petr Bosáková, Zuzana Tesařová, Eva Coufal, Pavel
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Univerzita Karlova v Praze / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	194026
http://linked.open...ai/riv/idVysledku	RIV/00216208:11310/11:10089764
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	WILDLIFE; FERTILITY; PROGESTOGENS; FATE; SLUDGE; SURFACE-WATER; MUNICIPAL SEWAGE; ELECTROSPRAY-IONIZATION; RIVER SEDIMENTS; ENDOCRINE-DISRUPTING CHEMICALS (en)
http://linked.open.../riv/klicoveSlovo	ELECTROSPRAY-IONIZATION ENDOCRINE-DISRUPTING CHEMICALS FATE FERTILITY MUNICIPAL SEWAGE PROGESTOGENS RIVER SEDIMENTS SLUDGE SURFACE-WATER WILDLIFE
http://linked.open...odStatuVydavatele	NL - Nizozemsko
http://linked.open...ontrolniKodProRIV	[56454648A756]
http://linked.open...i/riv/nazevZdroje	Journal of Chromatography A
http://linked.open...in/vavai/riv/obor	CB
http://linked.open...ichTvurcuVysledku	5 (xsd:int)
http://linked.open...cetTvurcuVysledku	5 (xsd:int)
http://linked.open...vavai/riv/projekt	The Centre of Molecular Methods for Monitoring the Diffuse Pollution of the Environment. Innovation of Laboratories of Advanced Separation Methods for Purposes of Whole-Life Education
http://linked.open...UplatneniVysledku	2011
http://linked.open...v/svazekPeriodika	1218
http://linked.open...iv/tvurceVysledku	Bosáková, Zuzana Coufal, Pavel Tesařová, Eva Čabala, Radomír Kozlík, Petr
http://linked.open...ain/vavai/riv/wos	000289331200025
http://linked.open...n/vavai/riv/zamer	Nové molekulární systémy pro pokročilé aplikace prospěšné pro zdraví a šetrné k životnímu prostředí
issn	0021-9673
number of pages	6 (xsd:int)
http://bibframe.org/vocab/doi	10.1016/j.chroma.2010.10.033
http://localhost/t...ganizacniJednotka	11310

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