About: Dissociation of nystatin and amphotericin analogues: characterisation of minor anti-fungal macrolides     Goto   Sponge   NotDistinct   Permalink

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Description
  • Tandem mass spectrometry combined with Fourier transform ion cyclotron resonance (FT-ICR) has been the basis for rationalizing the fragmentation mechanisms of anti-fungal macrolides nystatin A(1) amphotericin B and pimaricin. The positive ion mass spectra were not informative, however, the dissociation of deprotonated molecules Led to structurally significant ring-opened fragments. Using this approach of tandem FT-ICR mass spectrometry and electrospray ionisation coupled with high-performance Liquid chromatography (HPLC), 11 macrolide natural analogues or degradation products were characterised in the nystatin mixture.
  • Tandem mass spectrometry combined with Fourier transform ion cyclotron resonance (FT-ICR) has been the basis for rationalizing the fragmentation mechanisms of anti-fungal macrolides nystatin A(1) amphotericin B and pimaricin. The positive ion mass spectra were not informative, however, the dissociation of deprotonated molecules Led to structurally significant ring-opened fragments. Using this approach of tandem FT-ICR mass spectrometry and electrospray ionisation coupled with high-performance Liquid chromatography (HPLC), 11 macrolide natural analogues or degradation products were characterised in the nystatin mixture. (en)
Title
  • Dissociation of nystatin and amphotericin analogues: characterisation of minor anti-fungal macrolides
  • Dissociation of nystatin and amphotericin analogues: characterisation of minor anti-fungal macrolides (en)
skos:prefLabel
  • Dissociation of nystatin and amphotericin analogues: characterisation of minor anti-fungal macrolides
  • Dissociation of nystatin and amphotericin analogues: characterisation of minor anti-fungal macrolides (en)
skos:notation
  • RIV/00216208:11310/10:10116644!RIV12-MSM-11310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • I, P(LC07017), Z(AV0Z50200510)
http://linked.open...iv/cisloPeriodika
  • 1
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
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  • 254676
http://linked.open...ai/riv/idVysledku
  • RIV/00216208:11310/10:10116644
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  • amphotericin; nystatin; antibiotics (en)
http://linked.open.../riv/klicoveSlovo
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  • GB - Spojené království Velké Británie a Severního Irska
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  • [408C2C62DB05]
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  • European Journal of Mass Spectrometry
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  • 16
http://linked.open...iv/tvurceVysledku
  • Lemr, Karel
  • Novák, Petr
  • Ulrych, Aleš
  • Havlíček, Vladimír
  • Derrick, Peter J.
  • Adámek, František
http://linked.open...ain/vavai/riv/wos
  • 000274290200008
http://linked.open...n/vavai/riv/zamer
issn
  • 1469-0667
number of pages
http://bibframe.org/vocab/doi
  • 10.1255/ejms.1027
http://localhost/t...ganizacniJednotka
  • 11310
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