About: Amperometric detection of aminobiphenyls in HPLC using microcrystalline boron- doped diamond Film Electrode in %22Wall-Jet%22 and %22Thin-Layer%22 arrangement     Goto   Sponge   NotDistinct   Permalink

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Description
  • The study compares HPLC determination of 2-aminobiphenyl, 3-aminobiphenyl, and 4-aminobiphenyl using amperometric detection at a microcrystalline boron-doped diamond film electrode in thin-layer and wall-jet arrangement. Satisfactory separation of studied analytes was achieved at a ChiraDex column (Merck) with chemically bonded beta-cyclodextrin in mobile phase consisting of 0.01 mol L-1 acetate buffer, pH 5 : acetonitrile : methanol (40:30:30; v/v/v) with total analysis time of six minutes. The repeatabilities of the detector responses are satisfactory. Slightly wider linear dynamic range of calibration dependencies and lower detection limits in the 10-8 mol L-1 concentration range were achieved for the walljet arrangement.
  • The study compares HPLC determination of 2-aminobiphenyl, 3-aminobiphenyl, and 4-aminobiphenyl using amperometric detection at a microcrystalline boron-doped diamond film electrode in thin-layer and wall-jet arrangement. Satisfactory separation of studied analytes was achieved at a ChiraDex column (Merck) with chemically bonded beta-cyclodextrin in mobile phase consisting of 0.01 mol L-1 acetate buffer, pH 5 : acetonitrile : methanol (40:30:30; v/v/v) with total analysis time of six minutes. The repeatabilities of the detector responses are satisfactory. Slightly wider linear dynamic range of calibration dependencies and lower detection limits in the 10-8 mol L-1 concentration range were achieved for the walljet arrangement. (en)
Title
  • Amperometric detection of aminobiphenyls in HPLC using microcrystalline boron- doped diamond Film Electrode in %22Wall-Jet%22 and %22Thin-Layer%22 arrangement
  • Amperometric detection of aminobiphenyls in HPLC using microcrystalline boron- doped diamond Film Electrode in %22Wall-Jet%22 and %22Thin-Layer%22 arrangement (en)
skos:prefLabel
  • Amperometric detection of aminobiphenyls in HPLC using microcrystalline boron- doped diamond Film Electrode in %22Wall-Jet%22 and %22Thin-Layer%22 arrangement
  • Amperometric detection of aminobiphenyls in HPLC using microcrystalline boron- doped diamond Film Electrode in %22Wall-Jet%22 and %22Thin-Layer%22 arrangement (en)
skos:notation
  • RIV/00216208:11310/10:10061943!RIV11-MSM-11310___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(LC06035), S, V, Z(MSM0021620857)
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
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  • 246121
http://linked.open...ai/riv/idVysledku
  • RIV/00216208:11310/10:10061943
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  • aminobiphenyls; wall-jet arrangement; thinlayer arrangement; amperometric detection; HPLC; boron-doped diamond film electrode (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...ontrolniKodProRIV
  • [184B215E13E4]
http://linked.open...v/mistoKonaniAkce
  • Jetřichovice
http://linked.open...i/riv/mistoVydani
  • Ústí nad Labem
http://linked.open...i/riv/nazevZdroje
  • Sborník přednášek mezinárodní odborné konference XXX. Moderní Elektrochemické Metody, Jetřichovice 24. ? 28. května 2010
http://linked.open...in/vavai/riv/obor
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http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...iv/tvurceVysledku
  • Barek, Jiří
  • Pecková, Karolina
  • Maixnerová, Lucie
http://linked.open...vavai/riv/typAkce
http://linked.open...ain/vavai/riv/wos
  • 000283050900024
http://linked.open.../riv/zahajeniAkce
http://linked.open...n/vavai/riv/zamer
number of pages
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  • Best servis Ústí nad Labem
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  • 978-80-254-6710-7
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  • 11310
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