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rdf:type
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Description
| - RP-HPLC and non-aqueous CZE methods were evaluated for qualitative and quantitative analysis of esterified macrocyclic compounds of the DOTA family (DOTA = 1,4,7,10-tetraazacyclododecan-1,4,7,10-tetraacetic: acid). This group of compounds represents important reaction intermediates in synthesis of magnetic resonance contrast agents. Calibration curves in the concentration range from 1.0 x 10(-5) to 1.0 x 10(-3) mol/L were plotted and the experimental data were critically compared in terms of their repeatability, linearity, LOD and LOQ. The optimized methods were successfully applied to the analysis of a real reaction mixture without any further pretreatment.
- RP-HPLC and non-aqueous CZE methods were evaluated for qualitative and quantitative analysis of esterified macrocyclic compounds of the DOTA family (DOTA = 1,4,7,10-tetraazacyclododecan-1,4,7,10-tetraacetic: acid). This group of compounds represents important reaction intermediates in synthesis of magnetic resonance contrast agents. Calibration curves in the concentration range from 1.0 x 10(-5) to 1.0 x 10(-3) mol/L were plotted and the experimental data were critically compared in terms of their repeatability, linearity, LOD and LOQ. The optimized methods were successfully applied to the analysis of a real reaction mixture without any further pretreatment. (en)
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Title
| - Comparison of HPLC and CZE methods for analysis of DOTA-like esters - reaction intermediates in synthesis of magnetic resonance contrast agents
- Comparison of HPLC and CZE methods for analysis of DOTA-like esters - reaction intermediates in synthesis of magnetic resonance contrast agents (en)
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skos:prefLabel
| - Comparison of HPLC and CZE methods for analysis of DOTA-like esters - reaction intermediates in synthesis of magnetic resonance contrast agents
- Comparison of HPLC and CZE methods for analysis of DOTA-like esters - reaction intermediates in synthesis of magnetic resonance contrast agents (en)
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skos:notation
| - RIV/00216208:11310/10:10056957!RIV11-MSM-11310___
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http://linked.open...avai/riv/aktivita
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http://linked.open...avai/riv/aktivity
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http://linked.open...iv/cisloPeriodika
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http://linked.open...vai/riv/dodaniDat
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http://linked.open...aciTvurceVysledku
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http://linked.open.../riv/druhVysledku
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http://linked.open...iv/duvernostUdaju
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http://linked.open...titaPredkladatele
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http://linked.open...dnocenehoVysledku
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http://linked.open...ai/riv/idVysledku
| - RIV/00216208:11310/10:10056957
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http://linked.open...riv/jazykVysledku
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http://linked.open.../riv/klicovaSlova
| - acid; plasma; instrumentation; lanthanide complexes; liquid-chromatographic determination (en)
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http://linked.open.../riv/klicoveSlovo
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http://linked.open...odStatuVydavatele
| - GB - Spojené království Velké Británie a Severního Irska
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http://linked.open...ontrolniKodProRIV
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http://linked.open...i/riv/nazevZdroje
| - Journal of Separation Science
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http://linked.open...in/vavai/riv/obor
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http://linked.open...ichTvurcuVysledku
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http://linked.open...cetTvurcuVysledku
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http://linked.open...UplatneniVysledku
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http://linked.open...v/svazekPeriodika
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http://linked.open...iv/tvurceVysledku
| - Bosáková, Zuzana
- Coufal, Pavel
- Kubíček, Vojtěch
- Křížek, Tomáš
- Hamplová, Anna
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http://linked.open...ain/vavai/riv/wos
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http://linked.open...n/vavai/riv/zamer
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issn
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number of pages
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http://localhost/t...ganizacniJednotka
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