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  • An overview of the existing methods for minimization of the analysis time in gas chromatography (GC) is presented and a new system for fast temperature programming and very fast cooling down is evaluated. In this study, a system of coaxial tubes, a heating/cooling module (HC-M), was developed and studied with a capillary column placed inside the HC-M. The module itself was heated by a GC oven and cooled down by an external cooling medium. The HC-M was heated at rates of up to 330 degrees C min(-1) and cooled at the rate of 6000 degrees C min(-1). The GC system was prepared for the next run within a few seconds. The HC-M permits good separation reproducibility, comparable with that of a conventional GC, expressed in terms of relative retention times and peak areas of analytes reproducibilities. The HC-M can be used within any commercial gas chromatograph. (c) 2008 Institute of Chemistry, Slovak Academy of Sciences.
  • An overview of the existing methods for minimization of the analysis time in gas chromatography (GC) is presented and a new system for fast temperature programming and very fast cooling down is evaluated. In this study, a system of coaxial tubes, a heating/cooling module (HC-M), was developed and studied with a capillary column placed inside the HC-M. The module itself was heated by a GC oven and cooled down by an external cooling medium. The HC-M was heated at rates of up to 330 degrees C min(-1) and cooled at the rate of 6000 degrees C min(-1). The GC system was prepared for the next run within a few seconds. The HC-M permits good separation reproducibility, comparable with that of a conventional GC, expressed in terms of relative retention times and peak areas of analytes reproducibilities. The HC-M can be used within any commercial gas chromatograph. (c) 2008 Institute of Chemistry, Slovak Academy of Sciences. (en)
Title
  • Gas chromatography with ballistic heating and ultrafast cooling of column
  • Gas chromatography with ballistic heating and ultrafast cooling of column (en)
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  • Gas chromatography with ballistic heating and ultrafast cooling of column
  • Gas chromatography with ballistic heating and ultrafast cooling of column (en)
skos:notation
  • RIV/00216208:11310/08:10112580!RIV12-MSM-11310___
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  • 368943
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  • RIV/00216208:11310/08:10112580
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  • phenols; ultrafast cooling; very fast chromatography; fast temperature programming (en)
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  • SK - Slovenská republika
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  • [F231497A0772]
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  • Chemical Papers
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  • 62
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  • Ševčík, Jiří
  • Blaško, Jaroslav
  • Kubinec, Róbert
  • Ostrovský, Ivan
  • Soják, Ladislav
  • Jurdáková, Helena
  • Krkošová, Žofia
http://linked.open...ain/vavai/riv/wos
  • 000253753700002
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  • 0366-6352
number of pages
http://bibframe.org/vocab/doi
  • 10.2478/s11696-008-0002-6
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  • 11310
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