About: Two-column Sequential Injection Chromatography - New approach for fast and effective analysis and its comparison with gradient elution chromatography

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rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	This work presents novel approach in low-pressure chromatography flow systems - two-column Sequential Injection Chromatography (2-C SIC) and its comparison with gradient elution chromatography on the same instrument. The system was equipped with two different chromatographic columns (connected to selection valve in parallel design) for isocratic separation and determination of all components in composed anti-inflammatory pharmaceutical preparation (tablets). The sample was first injected on the first column of length 30mm where less retained analytes were separated and then the sample was injected on the second column of length 10mmwhere more retained analytes were separated. The new two-column chromatographic set-up shows evident advantages as compared with single-column gradient method. This work presents novel approach in low-pressure chromatography flow systems - two-column Sequential Injection Chromatography (2-C SIC) and its comparison with gradient elution chromatography on the same instrument. The system was equipped with two different chromatographic columns (connected to selection valve in parallel design) for isocratic separation and determination of all components in composed anti-inflammatory pharmaceutical preparation (tablets). The sample was first injected on the first column of length 30mm where less retained analytes were separated and then the sample was injected on the second column of length 10mmwhere more retained analytes were separated. The new two-column chromatographic set-up shows evident advantages as compared with single-column gradient method. (en)
Title	Two-column Sequential Injection Chromatography - New approach for fast and effective analysis and its comparison with gradient elution chromatography Two-column Sequential Injection Chromatography - New approach for fast and effective analysis and its comparison with gradient elution chromatography (en)
skos:prefLabel	Two-column Sequential Injection Chromatography - New approach for fast and effective analysis and its comparison with gradient elution chromatography Two-column Sequential Injection Chromatography - New approach for fast and effective analysis and its comparison with gradient elution chromatography (en)
skos:notation	RIV/00216208:11160/10:00300543!RIV11-GA0-11160___
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(GP203/08/P338), Z(MSM0021620822)
http://linked.open...iv/cisloPeriodika	1
http://linked.open...vai/riv/dodaniDat	2011
http://linked.open...aciTvurceVysledku	Chocholouš, Petr Šatínský, Dalibor Sklenářová, Hana Solich, Petr
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Univerzita Karlova v Praze / Farmaceutická fakulta v Hradci Králové
http://linked.open...dnocenehoVysledku	293889
http://linked.open...ai/riv/idVysledku	RIV/00216208:11160/10:00300543
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	sequential injection chromatography; two-column chromatography; monolithic column; paracetamol; caffeine; propyphenazone (en)
http://linked.open.../riv/klicoveSlovo	monolithic column caffeine paracetamol sequential injection chromatography propyphenazone two-column chromatography
http://linked.open...odStatuVydavatele	NL - Nizozemsko
http://linked.open...ontrolniKodProRIV	[421354D41367]
http://linked.open...i/riv/nazevZdroje	Analytica Chimica Acta
http://linked.open...in/vavai/riv/obor	FR
http://linked.open...ichTvurcuVysledku	4 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...vavai/riv/projekt	Using of monolithic column and LPME in sequential injection chromatography for drug analysis and biological samples pretreatment
http://linked.open...UplatneniVysledku	2010
http://linked.open...v/svazekPeriodika	668
http://linked.open...iv/tvurceVysledku	Sklenářová, Hana Solich, Petr Chocholouš, Petr Šatínský, Dalibor
http://linked.open...ain/vavai/riv/wos	000278306800011
http://linked.open...n/vavai/riv/zamer	Research of new drug structures
issn	0003-2670
number of pages	6 (xsd:int)
http://localhost/t...ganizacniJednotka	11160

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