About: Vapour generation inductively coupled plasma optical emission spectrometry in determination of total iodine in milk

Facets (new session)
Description
Metadata
Settings
- owl:sameAs
- Inference Rule:

About: Vapour generation inductively coupled plasma optical emission spectrometry in determination of total iodine in milk Goto Sponge NotDistinct Permalink

An Entity of Type : http://linked.opendata.cz/ontology/domain/vavai/Vysledek, within Data Space : linked.opendata.cz associated with source document(s)

Attributes	Values
rdf:type	skos:Concept http://linked.opendata.cz/ontology/domain/vavai/Vysledek
Description	Vapour generation inductively coupled plasma optical emission spectrometry (VG-ICP-OES) was used for the determination of the iodine content in milk samples. Modified alkaline ashing of the milk sample was employed for the total digestion of organic matrix constituents. A mixture of potassium hydroxide (2 mL, 2 mol L-1 in ethanol) and calcium nitrate (2 mL, 0.4 mol L-1 in ethanol) was used in the digestion step as an ashing aid for 2 ml of milk sample (or 200 mg of milk powder). Sample ash was then treated with hydrochloric acid (1.5 mL, 5 mol L-1) and sodium sulfite (1.25 mL, 1 mol L-1) for the elimination of carbonates, which would otherwise cause spectral interference. The vapour of elemental iodine was generated by means of oxidation of iodide by hydrogen peroxide (1 mol L-1) in sulfuric acid (5 mol L-1). Using a gas phase separator, matrix elements were completely eliminated; thus the spectral interference of phosphorus (178.222 nm) was removed and the most intense analytical line of iodine (178. Vapour generation inductively coupled plasma optical emission spectrometry (VG-ICP-OES) was used for the determination of the iodine content in milk samples. Modified alkaline ashing of the milk sample was employed for the total digestion of organic matrix constituents. A mixture of potassium hydroxide (2 mL, 2 mol L-1 in ethanol) and calcium nitrate (2 mL, 0.4 mol L-1 in ethanol) was used in the digestion step as an ashing aid for 2 ml of milk sample (or 200 mg of milk powder). Sample ash was then treated with hydrochloric acid (1.5 mL, 5 mol L-1) and sodium sulfite (1.25 mL, 1 mol L-1) for the elimination of carbonates, which would otherwise cause spectral interference. The vapour of elemental iodine was generated by means of oxidation of iodide by hydrogen peroxide (1 mol L-1) in sulfuric acid (5 mol L-1). Using a gas phase separator, matrix elements were completely eliminated; thus the spectral interference of phosphorus (178.222 nm) was removed and the most intense analytical line of iodine (178. (en)
Title	Vapour generation inductively coupled plasma optical emission spectrometry in determination of total iodine in milk Vapour generation inductively coupled plasma optical emission spectrometry in determination of total iodine in milk (en)
skos:prefLabel	Vapour generation inductively coupled plasma optical emission spectrometry in determination of total iodine in milk Vapour generation inductively coupled plasma optical emission spectrometry in determination of total iodine in milk (en)
skos:notation	RIV/00216224:14310/05:00012569!RIV10-MSM-14310___
http://linked.open...avai/riv/aktivita	P Z
http://linked.open...avai/riv/aktivity	P(GP203/03/D018), Z(MSM0021622411), Z(MSM0021622412)
http://linked.open...iv/cisloPeriodika	9
http://linked.open...vai/riv/dodaniDat	2010
http://linked.open...aciTvurceVysledku	Otruba, Vítězslav Niedobová, Eva Kanický, Viktor Machát, Jiří
http://linked.open.../riv/druhVysledku	J - Článek v odborném periodiku
http://linked.open...iv/duvernostUdaju	S - Úplné a pravdivé údaje nepodléhající ochraně podle zvláštních právních předpisů
http://linked.open...titaPredkladatele	Masarykova univerzita / Přírodovědecká fakulta
http://linked.open...dnocenehoVysledku	548498
http://linked.open...ai/riv/idVysledku	RIV/00216224:14310/05:00012569
http://linked.open...riv/jazykVysledku	eng - angličtina
http://linked.open.../riv/klicovaSlova	ICP optical emission spectrometry; vapour generation; iodine; milk (en)
http://linked.open.../riv/klicoveSlovo	ICP optical emission spectrometry milk iodine vapour generation
http://linked.open...odStatuVydavatele	US - Spojené státy americké
http://linked.open...ontrolniKodProRIV	[63F99C16F750]
http://linked.open...i/riv/nazevZdroje	Journal of Analytical Atomic Spectrometry
http://linked.open...in/vavai/riv/obor	CB
http://linked.open...ichTvurcuVysledku	4 (xsd:int)
http://linked.open...cetTvurcuVysledku	4 (xsd:int)
http://linked.open...vavai/riv/projekt	Generation of less common volatile compounds with optical emission spectrometry for determination of some elements and species
http://linked.open...UplatneniVysledku	2005
http://linked.open...v/svazekPeriodika	20
http://linked.open...iv/tvurceVysledku	Kanický, Viktor Otruba, Vítězslav Machát, Jiří Niedobová, Eva
http://linked.open...n/vavai/riv/zamer	Study and application of plasma chemical reactions in non-isothermic low temperature plasma and its interaction with solid surface Interactions among the chemicals, environment and biological systems and their consequences on the global, regional and local scales (INCHEMBIOL)
issn	0267-9477
number of pages	5 (xsd:int)
http://localhost/t...ganizacniJednotka	14310

Faceted Search & Find service v1.16.118 as of Jun 21 2024

Alternative Linked Data Documents: ODE Content Formats:

RDF

ODATA

Microdata

About

OpenLink Virtuoso version 07.20.3240 as of Jun 21 2024, on Linux (x86_64-pc-linux-gnu), Single-Server Edition (126 GB total memory, 112 GB memory in use)
Data on this page belongs to its respective rights holders.
Virtuoso Faceted Browser Copyright © 2009-2024 OpenLink Software