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  • The article reports on epsilon-Fe2O3 nanoparticles synthesized in a single step by atmospheric-pressure microwave torch discharge using gaseous precursors only. Morphology and composition of the as-synthesized nanopowder were studied by HR-TEM, XRD, and Mossbauer spectroscopy. In the studied nanopowder, epsilon-Fe2O3 phase (d(xRD)=25 nm, 32 wt%) together with alpha-Fe2O3 and gamma-Fe2O3 phases was found. The characteristic epsilon-Fe2O3 and alpha/gamma-Fe2O3 sextets in the Mossbauer spectra measured at 293 and 5 K confirmed the phase composition of the powder. Compared with the methods currently used for the synthesis of epsilon-Fe2O3 nanoparticles, atmospheric-pressure microwave torch discharge appears as a new synthesis route for obtaining epsilon-Fe2O3 nanoparticles. (C) 2013 Elsevier B.V. All rights reserved.
  • The article reports on epsilon-Fe2O3 nanoparticles synthesized in a single step by atmospheric-pressure microwave torch discharge using gaseous precursors only. Morphology and composition of the as-synthesized nanopowder were studied by HR-TEM, XRD, and Mossbauer spectroscopy. In the studied nanopowder, epsilon-Fe2O3 phase (d(xRD)=25 nm, 32 wt%) together with alpha-Fe2O3 and gamma-Fe2O3 phases was found. The characteristic epsilon-Fe2O3 and alpha/gamma-Fe2O3 sextets in the Mossbauer spectra measured at 293 and 5 K confirmed the phase composition of the powder. Compared with the methods currently used for the synthesis of epsilon-Fe2O3 nanoparticles, atmospheric-pressure microwave torch discharge appears as a new synthesis route for obtaining epsilon-Fe2O3 nanoparticles. (C) 2013 Elsevier B.V. All rights reserved. (en)
Title
  • epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch
  • epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch (en)
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  • epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch
  • epsilon-Fe2O3 nanoparticles synthesized in atmospheric-pressure microwave torch (en)
skos:notation
  • RIV/00216224:14740/14:00073662!RIV15-MSM-14740___
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • I, P(ED1.1.00/02.0068), P(ED2.1.00/03.0086), P(GA106/08/1440), P(GA202/08/0178), P(GAP205/10/1374), Z(AV0Z20410507)
http://linked.open...iv/cisloPeriodika
  • February
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  • 14886
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  • RIV/00216224:14740/14:00073662
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  • epsilon-Fe2O3; Nanoparticles; Microwave plasma; Mössbauer spectroscopy (en)
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  • NL - Nizozemsko
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  • [268B9CBD0FDF]
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  • Materials Letters
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  • 116
http://linked.open...iv/tvurceVysledku
  • David, Bohumil
  • Jašek, Ondřej
  • Kudrle, Vít
  • Schneeweiss, Oldřich
  • Pizúrová, Naděžda
  • Synek, Petr
http://linked.open...ain/vavai/riv/wos
  • 000331025500100
http://linked.open...n/vavai/riv/zamer
issn
  • 0167-577X
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.matlet.2013.11.057
http://localhost/t...ganizacniJednotka
  • 14740
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