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Description
  • Tato práce je zaměřena na přípravu nepolárních derivátů 1-monoacylglycerolů. Nejdříve byly adicí mastné kyseliny na glycidol vyrobeny monoacylglyceroly kyseliny laurové a olejové, následně pak azeotropní destilací v benzenu, za katalýzy kys. p-toluensulfonové, příslušné acetonidy. Kvalita produktů byla vždy testována pomocí TLC. Acetonid monolauroylglycerolu byl analyzován i pomocí IR spektroskopie. Dále byla testována stabilita acetonidů vůči hydrolýze. (cs)
  • The main aim of this work is preparation of not-polar derivates of 1-monoglycerides. At first monoglycerides of lauric and oleic acid were prepared by the addition of fatty acid to glycidol, than by azeotropic destilation in benzen, by p-toluensulfon acid katalysis, were prepared their acetonides. The quality of products was always tested by TLC chromatography. Acetonide of monolauroylglycerol was also analysed by IR spectroscopy. Also the stability of these acetonides was tested against hydrolysis.
  • The main aim of this work is preparation of not-polar derivates of 1-monoglycerides. At first monoglycerides of lauric and oleic acid were prepared by the addition of fatty acid to glycidol, than by azeotropic destilation in benzen, by p-toluensulfon acid katalysis, were prepared their acetonides. The quality of products was always tested by TLC chromatography. Acetonide of monolauroylglycerol was also analysed by IR spectroscopy. Also the stability of these acetonides was tested against hydrolysis. (en)
Title
  • Preparation of non-polar derivatives of 1-monoacylglycerols
  • Preparation of non-polar derivatives of 1-monoacylglycerols (en)
  • Příprava nepolárních derivátů 1-monoacylglycerolů (cs)
skos:prefLabel
  • Preparation of non-polar derivatives of 1-monoacylglycerols
  • Preparation of non-polar derivatives of 1-monoacylglycerols (en)
  • Příprava nepolárních derivátů 1-monoacylglycerolů (cs)
skos:notation
  • RIV/70883521:28110/07:63505463!RIV08-MSM-28110___
http://linked.open.../vavai/riv/strany
  • 1523-1526
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM7088352101)
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
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http://linked.open...iv/duvernostUdaju
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  • 443867
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  • RIV/70883521:28110/07:63505463
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  • Monoacylglycerol; Acetonides; Purification (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...ontrolniKodProRIV
  • [2EF9039485D8]
http://linked.open...i/riv/mistoVydani
  • Zenica
http://linked.open...i/riv/nazevZdroje
  • TMT2007 11th International research/expert conference %22Trends in the Development of Machinery and Associated Technology%22
http://linked.open...in/vavai/riv/obor
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http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...iv/tvurceVysledku
  • Janiš, Rahula
  • Krejčí, Jiří
  • Vltavská, P.
  • Bobálová, J.
http://linked.open...n/vavai/riv/zamer
number of pages
http://purl.org/ne...btex#hasPublisher
  • Faculty of Mechanical Engineering in Zenica
https://schema.org/isbn
  • 978-9958-617-34-8
http://localhost/t...ganizacniJednotka
  • 28110
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