About: 3,5-Dinitrosalicylic acid-assisted synthesis of self-assembled polyaniline nanorods     Goto   Sponge   Distinct   Permalink

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  • Self-assembled polyaniline nanorods were synthesized by the oxidation of aniline with ammonium peroxydisulfate in an aqueous solution in the presence of 3,5-dinitrosalicylic acid, using the template-free falling-pH method. The effects of the mole ratio of 3,5-dinitrosalicylic acid to aniline, i.e., of starting pH, monomer concentration, and reaction time on the yield of polymerization, molecular-weight distribution, molecular structure, morphology, and conductivity of the prepared polyanilines have been studied by gel-permeation chromatography, elemental analysis, FTIR and Raman spectroscopies, scanning and transmission electron microscopies, and conductivity measurements. The formation mechanism of self-assembled polyaniline nanorods has been discussed.
  • Self-assembled polyaniline nanorods were synthesized by the oxidation of aniline with ammonium peroxydisulfate in an aqueous solution in the presence of 3,5-dinitrosalicylic acid, using the template-free falling-pH method. The effects of the mole ratio of 3,5-dinitrosalicylic acid to aniline, i.e., of starting pH, monomer concentration, and reaction time on the yield of polymerization, molecular-weight distribution, molecular structure, morphology, and conductivity of the prepared polyanilines have been studied by gel-permeation chromatography, elemental analysis, FTIR and Raman spectroscopies, scanning and transmission electron microscopies, and conductivity measurements. The formation mechanism of self-assembled polyaniline nanorods has been discussed. (en)
Title
  • 3,5-Dinitrosalicylic acid-assisted synthesis of self-assembled polyaniline nanorods
  • 3,5-Dinitrosalicylic acid-assisted synthesis of self-assembled polyaniline nanorods (en)
skos:prefLabel
  • 3,5-Dinitrosalicylic acid-assisted synthesis of self-assembled polyaniline nanorods
  • 3,5-Dinitrosalicylic acid-assisted synthesis of self-assembled polyaniline nanorods (en)
skos:notation
  • RIV/61389013:_____/10:00346828!RIV11-GA0-61389013
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA203/08/0686), Z(AV0Z40500505)
http://linked.open...iv/cisloPeriodika
  • 21
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 301002
http://linked.open...ai/riv/idVysledku
  • RIV/61389013:_____/10:00346828
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • FTIR spectroscopy; nanorods; polyaniline (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [939D2FA2787C]
http://linked.open...i/riv/nazevZdroje
  • Materials Letters
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 64
http://linked.open...iv/tvurceVysledku
  • Ciric-Marjanovic, G.
  • Marjanovic, B.
  • Stejskal, Jaroslav
  • Trchová, Miroslava
  • Janoševic, A.
http://linked.open...ain/vavai/riv/wos
  • 000282907700019
http://linked.open...n/vavai/riv/zamer
issn
  • 0167-577X
number of pages
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