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  • Review sumarizuje přípravu a použití chromatografických separačních medií, založených na methakrylátových monomerech, s hlavním zaměřením na vysoko síťované makroporézní sférické částice připravené z 2-hydroxyethyl methakrylátu a glycidyl methakrylátu. Účinky proměnných procesu, jako jsou složení polymerizační směsi, které zahrnují monomer, porogen, radikálový iniciátor, stabilizátor suspenze, reakční teplota a míchání, jsou podrobně popsány pro klasickou i templátovou suspenzní polymerizaci. Kromě toho jsou také diskutovány specifické rysy přípravy monodisperzních sférických částic. Účinnost methakrylátových separačních medií je předvedena na řadě separací v různých chromatografických modech. (cs)
  • The review summarizes the preparation and application of chromatographic separation media based on methacrylate monomers with a major focus on highly crosslinked macroporous beads prepared from 2-hydroxyethyl methacrylate and glycidyl methacrylate, respectively. The effects of process variables such as composition of the polymerization mixture that includes monomers, porogenic solvents, and free radical initiator, suspension stabilizer, reaction temperature, and stirring are detailed for both classical and templated suspension polymerization. In addition, specific features of the preparation of monodisperse beads are also discussed. The performance of methacrylate-based separation media is demonstrated on numerous separations in a variety of chromatographic modes.
  • The review summarizes the preparation and application of chromatographic separation media based on methacrylate monomers with a major focus on highly crosslinked macroporous beads prepared from 2-hydroxyethyl methacrylate and glycidyl methacrylate, respectively. The effects of process variables such as composition of the polymerization mixture that includes monomers, porogenic solvents, and free radical initiator, suspension stabilizer, reaction temperature, and stirring are detailed for both classical and templated suspension polymerization. In addition, specific features of the preparation of monodisperse beads are also discussed. The performance of methacrylate-based separation media is demonstrated on numerous separations in a variety of chromatographic modes. (en)
Title
  • Methacrylate-based chromatographic media
  • Chromatografické nosiče na bázi methakrylátu (cs)
  • Methacrylate-based chromatographic media (en)
skos:prefLabel
  • Methacrylate-based chromatographic media
  • Chromatografické nosiče na bázi methakrylátu (cs)
  • Methacrylate-based chromatographic media (en)
skos:notation
  • RIV/61389013:_____/05:00021580!RIV06-GA0-61389013
http://linked.open.../vavai/riv/strany
  • 1855;1875
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA203/05/0241), P(GA525/05/0311)
http://linked.open...iv/cisloPeriodika
  • 15
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 529691
http://linked.open...ai/riv/idVysledku
  • RIV/61389013:_____/05:00021580
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • beads; characterization; chromatography (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • DE - Spolková republika Německo
http://linked.open...ontrolniKodProRIV
  • [5560856BC41D]
http://linked.open...i/riv/nazevZdroje
  • Journal of Separation Science
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...vavai/riv/projekt
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • 28
http://linked.open...iv/tvurceVysledku
  • Horák, Daniel
  • Beneš, Milan
  • Švec, F.
issn
  • 1615-9306
number of pages
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