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  • Iodine was determined in foodstuffs consumed in Libya employing two modes of NAA.The first mode was instrumental using short-time irradiation with epithermal neutrons behind a Cd shield(EINAA). The other mode utilized shor-time irradiation with the reactor-pile neutrons followed by radiochemical separation (RNAA). The radiochemical separation procedure was based on the alkaline-oxidative fusion of samples and extraction of elemental iodine into chloroform. Separation yield determined using the radiotracer131 I was within the range of 90 to 95%. For guality control purposes,standard reference materials were analyzed in both modes employed.Using RNAA, a decection limit of ~1 ng g -1 could be obtained indicating superiority of the method in measuring ultra-trace levels of iodine. On the other hand, more than one order of magnitude higher detection limit did not allow sufficiently accurate determination of iodine in Libyan foodstuffs using EINAA.
  • Iodine was determined in foodstuffs consumed in Libya employing two modes of NAA.The first mode was instrumental using short-time irradiation with epithermal neutrons behind a Cd shield(EINAA). The other mode utilized shor-time irradiation with the reactor-pile neutrons followed by radiochemical separation (RNAA). The radiochemical separation procedure was based on the alkaline-oxidative fusion of samples and extraction of elemental iodine into chloroform. Separation yield determined using the radiotracer131 I was within the range of 90 to 95%. For guality control purposes,standard reference materials were analyzed in both modes employed.Using RNAA, a decection limit of ~1 ng g -1 could be obtained indicating superiority of the method in measuring ultra-trace levels of iodine. On the other hand, more than one order of magnitude higher detection limit did not allow sufficiently accurate determination of iodine in Libyan foodstuffs using EINAA. (en)
  • Obsah jódu v potravinách konzumovaných v Libyi byl stanovován s použitím instrumentální a radiochemické neutronové aktivační analýzy (INAA a RNAA). Postup INAA byl založen na krátkodobé aktivaci v kadmiovém stínění, tj.aktivaci epitermálními neutrony. Postup RNAA byl založen na krátkodobé aktivaci celým spektrem neutronů a následné radiochemické separaci jódu sestávající z rozkladu vzorku alkalickým oxidačním tavením a extrakce elementárního jódu do chloroformu. Pro stanovení jódu v libyjských potravinách na úrovni ng/g se ukázalo nevyhnutelné použití RNAA, neboť mez detekce jódu metodou INAA byla minimálně o řád vyšší. (cs)
Title
  • Determination of iodine in foodstuffs consumed in Libya using instrumental and radiochemical neutro activation analysis
  • Stanovení jódu v potravinách konzumovaných v Libyi s použitím instrumentální a radiochemické neutronové aktavační analýzy (cs)
  • Determination of iodine in foodstuffs consumed in Libya using instrumental and radiochemical neutro activation analysis (en)
skos:prefLabel
  • Determination of iodine in foodstuffs consumed in Libya using instrumental and radiochemical neutro activation analysis
  • Stanovení jódu v potravinách konzumovaných v Libyi s použitím instrumentální a radiochemické neutronové aktavační analýzy (cs)
  • Determination of iodine in foodstuffs consumed in Libya using instrumental and radiochemical neutro activation analysis (en)
skos:notation
  • RIV/61389005:_____/06:00078918!RIV07-AV0-61389005
http://linked.open.../vavai/riv/strany
  • 159;163
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(AV0Z10480505)
http://linked.open...iv/cisloPeriodika
  • 56
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 471148
http://linked.open...ai/riv/idVysledku
  • RIV/61389005:_____/06:00078918
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • determination of iodine; neutron activation analysis (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • CZ - Česká republika
http://linked.open...ontrolniKodProRIV
  • [ECD3426CBBE9]
http://linked.open...i/riv/nazevZdroje
  • Czechoslovak Journal of Physics
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • -
http://linked.open...iv/tvurceVysledku
  • Kučera, Jan
  • Mizera, Jiří
  • Alamin, M. B.
  • Bejey, A. M.
http://linked.open...n/vavai/riv/zamer
issn
  • 0011-4626
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