About: Determination of Glycyrrhizin in liqueurs by on-line coupled capillary isotachophoresis with capillary zone electrophoresis     Goto   Sponge   Distinct   Permalink

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  • An on-line coupled capillary isotachophoresis-capillary zone electrophoresis method for the determination of glycyrrhizin in liqueurs is described. The optimised electrolyte system was 5mMHCl + 11mM_-aminocaproic acid + 0.05% hydroxyethylcellulose + 30% methanol (leasing electrolyte), 5mM caproic acid + 30% methanol (terminating electrolyte) and 20mM caproic acid + 10mM histidine + 0.1% hydroxyethylcellulose + 30% methanol (background electrolyte). Method characteristics, i.e., linearity (20-500 ng/ml), accuracy (recovery 99+/-4%), intra-assay repeatability (2%), intermediate repeatability (3.8%) and detection limit (8 ng/ml) were determined. Speed of analysis, low laboriousness, high sensitivity and low-running cost are the typical attributes of the capillary isotachophoresis-capillary zone electrophoresis method. Developed method was successfully applied to analysis of liqueurs with liquorice extract and some foods (sweets and food supplements) containing liquorice. Found levels of glycyrrhizin in l
  • An on-line coupled capillary isotachophoresis-capillary zone electrophoresis method for the determination of glycyrrhizin in liqueurs is described. The optimised electrolyte system was 5mMHCl + 11mM_-aminocaproic acid + 0.05% hydroxyethylcellulose + 30% methanol (leasing electrolyte), 5mM caproic acid + 30% methanol (terminating electrolyte) and 20mM caproic acid + 10mM histidine + 0.1% hydroxyethylcellulose + 30% methanol (background electrolyte). Method characteristics, i.e., linearity (20-500 ng/ml), accuracy (recovery 99+/-4%), intra-assay repeatability (2%), intermediate repeatability (3.8%) and detection limit (8 ng/ml) were determined. Speed of analysis, low laboriousness, high sensitivity and low-running cost are the typical attributes of the capillary isotachophoresis-capillary zone electrophoresis method. Developed method was successfully applied to analysis of liqueurs with liquorice extract and some foods (sweets and food supplements) containing liquorice. Found levels of glycyrrhizin in l (en)
  • An on-line coupled capillary isotachophoresis-capillary zone electrophoresis method for the determination of glycyrrhizin in liqueurs is described. The optimised electrolyte system was 5mMHCl + 11mM_-aminocaproic acid + 0.05% hydroxyethylcellulose + 30% methanol (leasing electrolyte), 5mM caproic acid + 30% methanol (terminating electrolyte) and 20mM caproic acid + 10mM histidine + 0.1% hydroxyethylcellulose + 30% methanol (background electrolyte). Method characteristics, i.e., linearity (20-500 ng/ml), accuracy (recovery 99+/-4%), intra-assay repeatability (2%), intermediate repeatability (3.8%) and detection limit (8 ng/ml) were determined. Speed of analysis, low laboriousness, high sensitivity and low-running cost are the typical attributes of the capillary isotachophoresis-capillary zone electrophoresis method. Developed method was successfully applied to analysis of liqueurs with liquorice extract and some foods (sweets and food supplements) containing liquorice. Found levels of glycyrrhizin in l (cs)
Title
  • Determination of Glycyrrhizin in liqueurs by on-line coupled capillary isotachophoresis with capillary zone electrophoresis
  • Stanovení glycyrrhizinu v lékérech kombinací CITP a CZE (cs)
  • Determination of Glycyrrhizin in liqueurs by on-line coupled capillary isotachophoresis with capillary zone electrophoresis (en)
skos:prefLabel
  • Determination of Glycyrrhizin in liqueurs by on-line coupled capillary isotachophoresis with capillary zone electrophoresis
  • Stanovení glycyrrhizinu v lékérech kombinací CITP a CZE (cs)
  • Determination of Glycyrrhizin in liqueurs by on-line coupled capillary isotachophoresis with capillary zone electrophoresis (en)
skos:notation
  • RIV/60461373:22330/07:00019024!RIV08-MSM-22330___
http://linked.open.../vavai/riv/strany
  • 239-242
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM6046137305)
http://linked.open...iv/cisloPeriodika
  • 1169
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
http://linked.open.../riv/druhVysledku
http://linked.open...iv/duvernostUdaju
http://linked.open...titaPredkladatele
http://linked.open...dnocenehoVysledku
  • 416659
http://linked.open...ai/riv/idVysledku
  • RIV/60461373:22330/07:00019024
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • glycyrrhizin; liqueur; liquorice; capillary; isotachophoresis; electrophoresis (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • BE - Belgické království
http://linked.open...ontrolniKodProRIV
  • [DA40AC398873]
http://linked.open...i/riv/nazevZdroje
  • Journal of Chromatography A
http://linked.open...in/vavai/riv/obor
http://linked.open...ichTvurcuVysledku
http://linked.open...cetTvurcuVysledku
http://linked.open...UplatneniVysledku
http://linked.open...iv/tvurceVysledku
  • Voldřich, Michal
  • Kvasnička, František
  • Vyhnálek, Josef
http://linked.open...n/vavai/riv/zamer
issn
  • 0021-9673
number of pages
http://localhost/t...ganizacniJednotka
  • 22330
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