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  • The aim of the study was to compare the properties of a new strong cation exchange-type (SCX) chiral stationary phase (CSP) in HPLC and SFC mode. We found that the new SCX CSP allows for effective enantiomer separation of variety of chiral amines in both HPLC and SFC mode. For some analytes we achieved higher efficiency of the column in the SFC mode. Additionally, we described properfies of in situ formed buffer species created upon reaction of supercritical CO2 with methanolic modifier containing a basic additive.
  • The aim of the study was to compare the properties of a new strong cation exchange-type (SCX) chiral stationary phase (CSP) in HPLC and SFC mode. We found that the new SCX CSP allows for effective enantiomer separation of variety of chiral amines in both HPLC and SFC mode. For some analytes we achieved higher efficiency of the column in the SFC mode. Additionally, we described properfies of in situ formed buffer species created upon reaction of supercritical CO2 with methanolic modifier containing a basic additive. (en)
Title
  • Strong cation exchange chiral stationary phase - A comparative study in high-performance liquid chromatography and subcritical fluid chromatography
  • Strong cation exchange chiral stationary phase - A comparative study in high-performance liquid chromatography and subcritical fluid chromatography (en)
skos:prefLabel
  • Strong cation exchange chiral stationary phase - A comparative study in high-performance liquid chromatography and subcritical fluid chromatography
  • Strong cation exchange chiral stationary phase - A comparative study in high-performance liquid chromatography and subcritical fluid chromatography (en)
skos:notation
  • RIV/60461373:22310/13:43896794!RIV14-MSM-22310___
http://linked.open...avai/predkladatel
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • S
http://linked.open...iv/cisloPeriodika
  • 22.11.2013
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
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  • 108282
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  • RIV/60461373:22310/13:43896794
http://linked.open...riv/jazykVysledku
http://linked.open.../riv/klicovaSlova
  • gradient elution; transient buffer salts; chiral cationion exchange; subcritical fluid chromatography; high-performance liquid chromatography; enantiomer separation (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [B792EEA9F1E3]
http://linked.open...i/riv/nazevZdroje
  • Journal of Chromatography A
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  • 1317
http://linked.open...iv/tvurceVysledku
  • Lindner, Wolfgang
  • Kohout, Michal
  • Macíková, Pavla
  • Wolrab, Denise
  • Boras, Mario
http://linked.open...ain/vavai/riv/wos
  • 000327229600008
issn
  • 0021-9673
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.chroma.2013.08.037
http://localhost/t...ganizacniJednotka
  • 22310
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