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  • Kinetika krystalizace amorfního TiO2 byla studována za neizotermních podmínek pomocí DSC. Bylo zjištěno, že tento proces může být popsán standardním Johnson-Mehl-Avrami-Kolmogorov (JMA) modelem s kinetickým exponentem m 1. Kinetické parametry byly vypočítány současnou analýzou experimentálních dat získaných při různých rychlostech ohřevu. Tyto parametry byly použity jako základní předpoklad pro kinetiku krystalizace za izotermních podmínek. Shoda mezi předpoklady JMA modelu a experimentálními daty závisí na metodě přípravy TiO2. (cs)
  • The kinetics of nanocrystallization in amorphous TiO2 has been studied in non-isothermal conditions by DSC. It was found that this process could be well described by standard Johnson-Mehl-Avrami-Kolmogorov (JMA) model with kinetic exponent m ?° 1. The kinetic parameters were calculated by simultaneous analysis of experimental data taken at different heating rates. These parameters were used as a basis for prediction of crystallization kinetics in isothermal conditions. The agreement between the JMA model prediction and experimental data depends on the method of preparation of amorphous TiO2.
  • The kinetics of nanocrystallization in amorphous TiO2 has been studied in non-isothermal conditions by DSC. It was found that this process could be well described by standard Johnson-Mehl-Avrami-Kolmogorov (JMA) model with kinetic exponent m ?° 1. The kinetic parameters were calculated by simultaneous analysis of experimental data taken at different heating rates. These parameters were used as a basis for prediction of crystallization kinetics in isothermal conditions. The agreement between the JMA model prediction and experimental data depends on the method of preparation of amorphous TiO2. (en)
Title
  • Nanocrystallization of anatase in amorphous TiO2
  • Nanocrystallization of anatase in amorphous TiO2 (en)
  • Nanokrystalizace anatasu v amorfním TiO2 (cs)
skos:prefLabel
  • Nanocrystallization of anatase in amorphous TiO2
  • Nanocrystallization of anatase in amorphous TiO2 (en)
  • Nanokrystalizace anatasu v amorfním TiO2 (cs)
skos:notation
  • RIV/00216275:25310/04:00001606!RIV08-MSM-25310___
http://linked.open.../vavai/riv/strany
  • 137-142
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • Z(MSM 253100001)
http://linked.open...iv/cisloPeriodika
  • 414
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  • 575299
http://linked.open...ai/riv/idVysledku
  • RIV/00216275:25310/04:00001606
http://linked.open...riv/jazykVysledku
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  • amorphous TiO2; crystallization kinetics; thermal analysis (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • NL - Nizozemsko
http://linked.open...ontrolniKodProRIV
  • [3E81F0F3A65F]
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  • Termochim. Acta
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http://linked.open...ichTvurcuVysledku
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http://linked.open...UplatneniVysledku
http://linked.open...v/svazekPeriodika
  • N.
http://linked.open...iv/tvurceVysledku
  • Málek, Jiří
  • Shánělová, Jana
  • Švadlák, Daniel
  • Criado, J.
  • Mitsuhashi, T.
  • Pérez-Maqueda, L.
http://linked.open...n/vavai/riv/zamer
issn
  • 0040-6031
number of pages
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  • 25310
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