About: Inclusion complexes between 3,3-substituted [n]staffanes and b-cyclodextrin in water.     Goto   Sponge   Distinct   Permalink

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  • Axially substituted [n]staffanes I form inclusion complexes with beta-cyclodextrin (II) in water. 1H NMR spectrum of a water solution of â-cyclodextrin II has shown apparent changes of chemical shifts of intracavity protons H-3 and H-5 upon addition of [2]staffane-3,3-diol (Ia)into the solution. Nuclear Overhauser effect has been observed between beta-cyclodextrin protons H-3, H-5 and bridge protons of the diol Ia. The method of continuous variations applied to the both complexation sensitive chemical shifts revealed formation of host-guest complex of 1:1 stoichiometry.
  • Axially substituted [n]staffanes I form inclusion complexes with beta-cyclodextrin (II) in water. 1H NMR spectrum of a water solution of â-cyclodextrin II has shown apparent changes of chemical shifts of intracavity protons H-3 and H-5 upon addition of [2]staffane-3,3-diol (Ia)into the solution. Nuclear Overhauser effect has been observed between beta-cyclodextrin protons H-3, H-5 and bridge protons of the diol Ia. The method of continuous variations applied to the both complexation sensitive chemical shifts revealed formation of host-guest complex of 1:1 stoichiometry. (en)
  • Axially substituted [n]staffanes I form inclusion complexes with â-cyclodextrin (II) in water. 1H NMR spectrum of a water solution of beta-cyclodextrin II has shown apparent changes of chemical shifts of intracavity protons H-3 and H-5 upon addition of [2]staffane-3,3-diol (Ia)into the solution. Nuclear Overhauser effect has been observed between beta-cyclodextrin protons H-3, H-5 and bridge protons of the diol Ia. The method of continuous variations applied to the both complexation sensitive chemical shifts revealed formation of host-guest complex of 1:1 stoichiometry. (cs)
Title
  • Inclusion complexes between 3,3-substituted [n]staffanes and b-cyclodextrin in water.
  • Inclusion complexes between 3,3-substituted [n]staffanes and b-cyclodextrin in water. (en)
  • Inclusion complexes between 3,3-substituted [n]staffanes and b-cyclodextrin in water. (cs)
skos:prefLabel
  • Inclusion complexes between 3,3-substituted [n]staffanes and b-cyclodextrin in water.
  • Inclusion complexes between 3,3-substituted [n]staffanes and b-cyclodextrin in water. (en)
  • Inclusion complexes between 3,3-substituted [n]staffanes and b-cyclodextrin in water. (cs)
skos:notation
  • RIV/00216224:14310/04:00010947!RIV09-MSM-14310___
http://linked.open...avai/riv/aktivita
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  • P(ME 571), Z(MSM 143100011)
http://linked.open...vai/riv/dodaniDat
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  • 567643
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  • RIV/00216224:14310/04:00010947
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  • bicyclopentanes; staffanes; cyclodextrin; NMR (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...ontrolniKodProRIV
  • [59A6A69964D7]
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  • Praha
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  • Praha
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  • Chemické listy
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  • Mazal, Ctibor
  • Bartoš, Petr
http://linked.open...vavai/riv/typAkce
http://linked.open.../riv/zahajeniAkce
http://linked.open...n/vavai/riv/zamer
issn
  • 0009-2770
number of pages
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  • Česká společnost chemická
http://localhost/t...ganizacniJednotka
  • 14310
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