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Description
| - This paper deals with a simple and low-cost method developed to deposit hematite (alfa-Fe2O3) layers on a fluorine-doped tin oxide (FTO/F:SnO2) substrate by thermal decomposition of solid iron(III) chloride hexahydrate (FeCl3?6H2O). Deposition procedure takes place through chemical intermediate iron(III) oxide chloride (FeOCl) film. A crucial influence of atmosphere dynamics involved in the calcination process of FeOCl has been observed. As-deposited films were characterized by means of Conversion Electron Mössbauer Spectroscopy (CEMS), Grazing Angle X-Ray Diffractometry (GAXRD), Atomic Force Microscopy (AFM), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray (EDX) analysis. Final nanocrystalline hematite film with a cactus-field-like design consists of 20 nm thick porous crystal plates. A process of hematite doping by tin atoms from substrate coating is also discussed.
- This paper deals with a simple and low-cost method developed to deposit hematite (alfa-Fe2O3) layers on a fluorine-doped tin oxide (FTO/F:SnO2) substrate by thermal decomposition of solid iron(III) chloride hexahydrate (FeCl3?6H2O). Deposition procedure takes place through chemical intermediate iron(III) oxide chloride (FeOCl) film. A crucial influence of atmosphere dynamics involved in the calcination process of FeOCl has been observed. As-deposited films were characterized by means of Conversion Electron Mössbauer Spectroscopy (CEMS), Grazing Angle X-Ray Diffractometry (GAXRD), Atomic Force Microscopy (AFM), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray (EDX) analysis. Final nanocrystalline hematite film with a cactus-field-like design consists of 20 nm thick porous crystal plates. A process of hematite doping by tin atoms from substrate coating is also discussed. (en)
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Title
| - A nanocrystalline hematite film prepared from iron(III) chloride precursor
- A nanocrystalline hematite film prepared from iron(III) chloride precursor (en)
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skos:prefLabel
| - A nanocrystalline hematite film prepared from iron(III) chloride precursor
- A nanocrystalline hematite film prepared from iron(III) chloride precursor (en)
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skos:notation
| - RIV/61989592:15310/10:10215253!RIV11-MSM-15310___
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http://linked.open...avai/riv/aktivita
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http://linked.open...avai/riv/aktivity
| - P(1M0512), P(KAN101630651), Z(MSM6198959218)
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http://linked.open...iv/cisloPeriodika
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http://linked.open...vai/riv/dodaniDat
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http://linked.open...aciTvurceVysledku
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http://linked.open.../riv/druhVysledku
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http://linked.open...iv/duvernostUdaju
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http://linked.open...titaPredkladatele
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http://linked.open...dnocenehoVysledku
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http://linked.open...ai/riv/idVysledku
| - RIV/61989592:15310/10:10215253
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http://linked.open...riv/jazykVysledku
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http://linked.open.../riv/klicovaSlova
| - Nanostructures; Mössbauer spectroscopy; Iron oxide; Hydrogen; Heat treatment; Deposition process (en)
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http://linked.open.../riv/klicoveSlovo
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http://linked.open...odStatuVydavatele
| - CH - Švýcarská konfederace
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http://linked.open...ontrolniKodProRIV
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http://linked.open...i/riv/nazevZdroje
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http://linked.open...in/vavai/riv/obor
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http://linked.open...ichTvurcuVysledku
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http://linked.open...cetTvurcuVysledku
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http://linked.open...vavai/riv/projekt
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http://linked.open...UplatneniVysledku
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http://linked.open...v/svazekPeriodika
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http://linked.open...iv/tvurceVysledku
| - Heřmánek, Martin
- Pechoušek, Jiří
- Sharma, Virender K.
- Tuček, Jiří
- Frydrych, Jiří
- Mašláň, Miroslav
- Machala, Libor
- Medřík, Ivo
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http://linked.open...ain/vavai/riv/wos
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http://linked.open...n/vavai/riv/zamer
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issn
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number of pages
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http://localhost/t...ganizacniJednotka
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