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  • Titanium(IV)-manganese(IV) nano-dispersed oxides were prepared by a homogeneous hydrolysis of potassium permanganate and titanium(IV) oxo-sulphate with 2-chloroacetamide. Synthesised samples were characterised using Brunauer-Emmett-Teller (BET) surface area and Barrett-Joiner-Halenda porosity (BJH), X-ray diffraction (XRD), infrared spectroscopy (IR), and scanning electron microscopy (SEM). These oxides were taken for an experimental evaluation of their reactivity with sulphur mustard (HD or bis(2-chloroethyl)sulphide) and soman (GD or (3,3'-dimethylbutan-2-yl)-methylphosphono-fluoridate). Mn(4+) content affects the decontamination activity; with increasing Mn(4+) content the activity increases for sulphur mustard and decreases for soman. The best decontamination activities for sulphur mustard and soman were observed for samples TiMn_37 with 18.6 wt.% Mn and TiMn_5 with 2.1 wt.% Mn, respectively.
  • Titanium(IV)-manganese(IV) nano-dispersed oxides were prepared by a homogeneous hydrolysis of potassium permanganate and titanium(IV) oxo-sulphate with 2-chloroacetamide. Synthesised samples were characterised using Brunauer-Emmett-Teller (BET) surface area and Barrett-Joiner-Halenda porosity (BJH), X-ray diffraction (XRD), infrared spectroscopy (IR), and scanning electron microscopy (SEM). These oxides were taken for an experimental evaluation of their reactivity with sulphur mustard (HD or bis(2-chloroethyl)sulphide) and soman (GD or (3,3'-dimethylbutan-2-yl)-methylphosphono-fluoridate). Mn(4+) content affects the decontamination activity; with increasing Mn(4+) content the activity increases for sulphur mustard and decreases for soman. The best decontamination activities for sulphur mustard and soman were observed for samples TiMn_37 with 18.6 wt.% Mn and TiMn_5 with 2.1 wt.% Mn, respectively. (en)
Title
  • Mesoporous titanium-manganese dioxide for sulphur mustard and soman decontamination
  • Mesoporous titanium-manganese dioxide for sulphur mustard and soman decontamination (en)
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  • Mesoporous titanium-manganese dioxide for sulphur mustard and soman decontamination
  • Mesoporous titanium-manganese dioxide for sulphur mustard and soman decontamination (en)
skos:notation
  • RIV/61388980:_____/11:00370934!RIV12-AV0-61388980
http://linked.open...avai/riv/aktivita
http://linked.open...avai/riv/aktivity
  • P(GA203/08/0334), Z(AV0Z40320502)
http://linked.open...iv/cisloPeriodika
  • 11
http://linked.open...vai/riv/dodaniDat
http://linked.open...aciTvurceVysledku
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http://linked.open...iv/duvernostUdaju
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  • 211650
http://linked.open...ai/riv/idVysledku
  • RIV/61388980:_____/11:00370934
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  • oxides; chemical synthesis; X-Ray diffraction; raman spectroscopy; infrared spectroscopy (en)
http://linked.open.../riv/klicoveSlovo
http://linked.open...odStatuVydavatele
  • GB - Spojené království Velké Británie a Severního Irska
http://linked.open...ontrolniKodProRIV
  • [3B5D88059DCB]
http://linked.open...i/riv/nazevZdroje
  • Materials Research Bulletin
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http://linked.open...ichTvurcuVysledku
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http://linked.open...vavai/riv/projekt
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http://linked.open...v/svazekPeriodika
  • 46
http://linked.open...iv/tvurceVysledku
  • Bludská, Jana
  • Štengl, Václav
  • Němec, T.
  • Opluštil, F.
http://linked.open...ain/vavai/riv/wos
  • 000296038700053
http://linked.open...n/vavai/riv/zamer
issn
  • 0025-5408
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.materresbull.2011.07.003
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