About: Microstructure stability of ultra-fine grained magnesium alloy AZ31 processed by extrusion and equal-channel angular pressing (EX-ECAP)     Goto   Sponge   Distinct   Permalink

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Description
  • Thermal stability of the ultra-fine grained (UFG) microstructure of magnesium AZ31 alloy was investigated. UFG microstructure was achieved by a combined two-step severe plastic deformation process: the extrusion (EX) and subsequent equal-channel angular pressing (ECAP). This combined process leads to refined microstructure and enhanced microhardness. Specimens with UFG microstructure were annealed isochronally at temperatures 150-500 degrees C for 1 h. The evolution of microstructure, mechanical properties and dislocation density was studied by electron backscatter diffraction (EBSD), microhardness measurements and positron annihilation spectroscopy (PAS). The coarsening of the fine-grained structure at higher temperatures was accompanied by a gradual decrease of the microhardness and decrease of dislocation density. Mechanism of grain growth was studied by general equation for grain growth and Arrhenius equation. Activation energies for grain growth were calculated to be 115, 33 and 164 kJ/mol in temperature ranges of 170-210 degrees C, 210-400 degrees C and 400-500 degrees C (443-483 K, 483-673 K and 673-773 K), respectively.
  • Thermal stability of the ultra-fine grained (UFG) microstructure of magnesium AZ31 alloy was investigated. UFG microstructure was achieved by a combined two-step severe plastic deformation process: the extrusion (EX) and subsequent equal-channel angular pressing (ECAP). This combined process leads to refined microstructure and enhanced microhardness. Specimens with UFG microstructure were annealed isochronally at temperatures 150-500 degrees C for 1 h. The evolution of microstructure, mechanical properties and dislocation density was studied by electron backscatter diffraction (EBSD), microhardness measurements and positron annihilation spectroscopy (PAS). The coarsening of the fine-grained structure at higher temperatures was accompanied by a gradual decrease of the microhardness and decrease of dislocation density. Mechanism of grain growth was studied by general equation for grain growth and Arrhenius equation. Activation energies for grain growth were calculated to be 115, 33 and 164 kJ/mol in temperature ranges of 170-210 degrees C, 210-400 degrees C and 400-500 degrees C (443-483 K, 483-673 K and 673-773 K), respectively. (en)
Title
  • Microstructure stability of ultra-fine grained magnesium alloy AZ31 processed by extrusion and equal-channel angular pressing (EX-ECAP)
  • Microstructure stability of ultra-fine grained magnesium alloy AZ31 processed by extrusion and equal-channel angular pressing (EX-ECAP) (en)
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  • Microstructure stability of ultra-fine grained magnesium alloy AZ31 processed by extrusion and equal-channel angular pressing (EX-ECAP)
  • Microstructure stability of ultra-fine grained magnesium alloy AZ31 processed by extrusion and equal-channel angular pressing (EX-ECAP) (en)
skos:notation
  • RIV/00216208:11320/14:10286337!RIV15-MSM-11320___
http://linked.open...avai/riv/aktivita
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  • I, P(GA13-13616S), S
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  • 29274
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  • RIV/00216208:11320/14:10286337
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  • AZ31 magnesium alloy; Equal-channel angular pressing (ECAP); Ultrafine-grained (UFG) materials; Severe plastic deformation (SPD); Microstructure stability (en)
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  • US - Spojené státy americké
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  • [C92A79A5DBB4]
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  • Materials Characterization
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  • 94
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  • Janeček, Miloš
  • Čížek, Jakub
  • Stráský, Josef
  • Hadzima, Branislav
  • Stráská, Jitka
http://linked.open...ain/vavai/riv/wos
  • 000339696000009
issn
  • 1044-5803
number of pages
http://bibframe.org/vocab/doi
  • 10.1016/j.matchar.2014.05.013
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  • 11320
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