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Description
  • The main aim of this project is an implementation and interlaboratory validation of analytical method applicable for a control of multiple residues of modern pesticieds in fruits, vegetables and grains. Performance parameters of this method enable the enforcement of EU maximum residue limits (MRLs) for respective commodities. Multiresidue method insists in utilization of ethyl acetate for extraction of residues from particular crop and subsequent purification of crude extract by gel permeation chromatography on Pl gel employing cyclohexane - ethyl acetate (1:1, v/v) as a mobile phase. Gas chromatography utilizing electron capture detector (ECD) and/or nitrogen-phosphorous detector (NPD) detector is used for quantitation of residues. Mass selective detector (MSD) is employed for confirmation purposes. (en)
  • Předmětem projektu je mezilaboratorní studie dvou CEN multireziduálních metod určených ke stanovení reziduí pesticidů v ovoci, zelenině a zrnech cereálií. Po ukončení procesu validace bude metoda využita ke kontrole dodržování hygienických limitů v EU. V prvé fázi projektu participující laboratoře provedly stanovení neznámých koncentrací vybraných pesticidů v testovacích roztocích a potravinářských materiálech za optimalizovaných GC podmínek. Diskuze výsledků proběhne na navazující %22project meeting%22.
Title
  • Collaborative study of two CEN multiresidue methods for the enforcement of EU MRLs for pesticide residues in fruits, vegetables and grains (en)
  • Mezilaboratorní studie dvou CEN multireziduálních metod pro prosazení hygienických limitů EU pro rezidua pesticidů v ovoci, zelenině a zrninách
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  • modern pesticides, food contaminants, multiresidue method, interlaboratory study, validation of anal (en)
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  • food contaminants
  • interlaboratory study
  • multiresidue method
  • modern pesticides
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